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Acta Cryst. (2013). E69, o1085  [ doi:10.1107/S1600536813015407 ]

2-{(E)-[(2-Methyl-3-nitrophenyl)imino]methyl}-4-nitrophenol

H. Tanak, F. Togurman, S. Kalecik, N. Dege and M. Yavuz


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B RINTA01_ALERT_3_B The value of Rint is greater than 0.18 Rint given 0.181 PLAT020_ALERT_3_B The value of Rint is greater than 0.12 ......... 0.181 PLAT026_ALERT_3_B Ratio Observed / Unique Reflections too Low .... 36 %
Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.974 PLAT147_ALERT_1_C su on Symmetry Constrained Cell Angle(s) ....... ? Check PLAT148_ALERT_3_C su on the a - Axis is (Too) Large ........ 0.005 Ang. PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for N1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for N3 PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0100 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 75.266 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.468 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 14.084 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.235 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 5.149 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.867 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 46
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT007_ALERT_5_G Note: Number of Unrefined Donor-H Atoms ........ 1 PLAT153_ALERT_1_G The su's on the Cell Axes are Equal .......... 0.00500 Ang. PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C14 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 22
0 ALERT level A = Most likely a serious problem - resolve or explain 3 ALERT level B = A potentially serious problem, consider carefully 13 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 13 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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