Acta Crystallographica Section E

Structure Reports Online

Volume 69, Part 7 (July 2013)

organic compounds

Acta Cryst. (2013). E69, o1147    [ doi:10.1107/S1600536813016954 ]

1,5-Bis(2-meth­oxy­benzyl­idene)thio­carbonohydrazide methanol monosolvate

J. Yu, S. Tang, J. Zeng and Z. Yan

Abstract: The title compound, C17H18N4O2S·CH3OH, was synthesized by the condensation reaction of o-meth­oxy­benzaldehyde with thio­carbohydrazide in methanol. The two benzene rings are inclined each to other at 31.7 (1)°. Inter­molecular N-H...O and bifurcated O-H...N(S) hydrogen bonds link two thio­carbonohydrazide and two solvent mol­ecules into a centrosymmetric unit. These units, related by translation along the b axis, are further aggregated into columns through N-H...S hydrogen bonds.

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