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Acta Cryst. (2013). E69, o1160-o1161  [ doi:10.1107/S1600536813017091 ]

N'-[(E)-4-Benzyloxy-2-hydroxybenzylidene]-4-nitrobenzohydrazide dimethylformamide monosolvate

B. Joseph, M. Sithambaresan and M. R. P. Kurup


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Alert level B PLAT919_ALERT_3_B Reflection # Likely Affected by the Beamstop ... 1 PLAT939_ALERT_3_B Large Value of Not (SHELXL) Weight Optimized S . 172.42
Alert level C PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for N3 PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of N4 PLAT334_ALERT_2_C Small Average Benzene C-C Dist. C16 -C21 1.37 Ang. PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -2.795 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 33 PLAT918_ALERT_3_C Reflection(s) # with I(obs) much smaller I(calc) 1 PLAT934_ALERT_3_C Number of (Iobs-Icalc)/SigmaW > 10 Outliers .... 1
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 4 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 2 C3 H7 N O PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 2 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 36
0 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 7 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 7 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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