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Acta Cryst. (2013). E69, o1162-o1163  [ doi:10.1107/S1600536813017054 ]

(3R*,6R*,4'S*,8'R*,3''R*,6''R*)-3,3''-Diisopropyl-6,6''-dimethyl-2',6'-diphenyldispiro[cyclohexane-1,4'-(3,7-dioxa-2,6-diazabicyclo[3.3.0]octane)-8',1''-cyclohexane]-2,2''-dione

A. Ansari, L. Majidi, R. Fihi, J.-C. Daran and M. Azrour


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Alert level C PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.3 Ratio PLAT230_ALERT_2_C Hirshfeld Test Diff for C42 -- C43 .. 5.5 su PLAT410_ALERT_2_C Short Intra H...H Contact H2 .. H32 .. 1.96 Ang. PLAT410_ALERT_2_C Short Intra H...H Contact H3 .. H26 .. 1.93 Ang. PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 7
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT791_ALERT_4_G Note: The Model has Chirality at C1 (Verify) R PLAT791_ALERT_4_G Note: The Model has Chirality at C2 (Verify) R PLAT791_ALERT_4_G Note: The Model has Chirality at C3 (Verify) R PLAT791_ALERT_4_G Note: The Model has Chirality at C4 (Verify) R PLAT791_ALERT_4_G Note: The Model has Chirality at C12 (Verify) R PLAT791_ALERT_4_G Note: The Model has Chirality at C15 (Verify) R PLAT791_ALERT_4_G Note: The Model has Chirality at C42 (Verify) R PLAT791_ALERT_4_G Note: The Model has Chirality at C45 (Verify) R
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 9 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 8 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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