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Acta Cryst. (2013). E69, o1035  [ doi:10.1107/S1600536813015213 ]

Methyl 11,14,16-triphenyl-8,12-dioxa-14,15-diazatetracyclo[8.7.0.02,7.013,17]heptadeca-2(7),3,5,13(17),15-pentaene-10-carboxylate

J. Kanchanadevi, G. Anbalagan, D. Kannan, B. Gunasekaran, V. Manivannan and N. Bakthadoss


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Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.979 PLAT230_ALERT_2_C Hirshfeld Test Diff for C15 -- C32 .. 5.7 su PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of . 36 Ang3 PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -0.385 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 3 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.597 90 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT128_ALERT_4_G Note: Alternate Setting of Space-group P21/c . P21/n PLAT153_ALERT_1_G The su's on the Cell Axes are Equal .......... 0.00500 Ang. PLAT793_ALERT_4_G The Model has Chirality at C8 (Verify) .... R PLAT793_ALERT_4_G The Model has Chirality at C15 (Verify) .... R PLAT793_ALERT_4_G The Model has Chirality at C23 (Verify) .... R PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 39 %
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 7 ALERT level C = Check. Ensure it is not caused by an omission or oversight 7 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check
checkCIF publication errors
Alert level A PUBL024_ALERT_1_A The number of authors is greater than 5. Please specify the role of each of the co-authors for your paper.
1 ALERT level A = Data missing that is essential or data in wrong format 0 ALERT level G = General alerts. Data that may be required is missing

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