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Acta Cryst. (2013). E69, m425  [ doi:10.1107/S1600536813017224 ]

Bis([mu]-6-methoxy-2-{[(3-oxidopropyl)imino]methyl}phenolato)nickel(II) methanol monosolvate

F.-K. Meng, X. Zhang, H. Yi, D.-H. Zhang and J.-Y. Jia


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Alert level C PLAT480_ALERT_4_C Long H...A H-Bond Reported H7 .. O3 .. 2.64 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 8.159 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.004 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 7 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 7 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1 PLAT973_ALERT_2_C Large Calcd. Positive Residual Density on Ni2 1.27 eA-3 PLAT976_ALERT_2_C Negative Residual Density at 0.88A from O2 . -0.60 eA-3
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 2 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ni1 -- O1 .. 6.0 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ni1 -- O5 .. 5.6 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ni1 -- N1 .. 6.7 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ni2 -- N2 .. 6.3 su PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 1 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 34
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 8 ALERT level C = Check. Ensure it is not caused by an omission or oversight 8 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 7 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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