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Acta Cryst. (2013). E69, m414-m415  [ doi:10.1107/S1600536813016309 ]

catena-Poly[[silver(I)-[mu]-N-(pyridin-3-ylmethyl)pyridine-2-amine-[kappa]2N:N'] trifluoromethanesulfonate]

S.-H. Moon and K.-M. Park


Key indicators

checkCIF/PLATON results

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Alert level C PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O5 PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0167 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 8.799 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.174 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 3 PLAT971_ALERT_2_C Large Calcd. Non-Metal Positive Residual Density 1.88 eA-3 PLAT971_ALERT_2_C Large Calcd. Non-Metal Positive Residual Density 1.61 eA-3 PLAT972_ALERT_2_C Large Calcd. Non-Metal Negative Residual Density -2.04 eA-3 PLAT972_ALERT_2_C Large Calcd. Non-Metal Negative Residual Density -1.79 eA-3
Alert level G PLAT003_ALERT_2_G Number of Uiso or Uij Restrained non-H Atoms ... 1 PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 2 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT007_ALERT_5_G Note: Number of Unrefined Donor-H Atoms ........ 2 PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? Check PLAT045_ALERT_1_G Calculated and Reported Z Differ by ............ 0.50 Ratio PLAT072_ALERT_2_G SHELXL First Parameter in WGHT Unusually Large. 0.13 PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 38.03 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 5 N2 -AG1 -N1 -C1 110.00 3.00 2.655 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 7 N2 -AG1 -N1 -C5 -67.00 3.00 2.655 1.555 1.555 1.555 PLAT793_ALERT_4_G The Model has Chirality at S1 (Verify) .... R PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 6
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 9 ALERT level C = Check. Ensure it is not caused by an omission or oversight 12 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 8 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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