# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' SK3-a at 296 K in P-1 (# 2 in standard setting)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 395.09 _exptl_crystal_F_000 1236.00 _reflns_d_resolution_high 0.7000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.7857 _cell_length_b 13.7658 _cell_length_c 17.0297 _cell_angle_alpha 66.581 _cell_angle_beta 78.689 _cell_angle_gamma 72.601 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4290.24 4983.13 49.84 o 3 0 0 1201.11 1519.78 37.74 o 4 0 0 35308.56 37179.71 731.56 o 5 0 0 6637.86 7096.42 116.11 o 6 0 0 2255.08 2285.50 121.03 o 7 0 0 1399.16 1336.93 105.23 o 8 0 0 2870.98 3116.44 126.22 o 9 0 0 31.83 8.48 123.09 o 10 0 0 403.39 338.81 142.49 o 11 0 0 426.49 447.79 162.83 o 12 0 0 769.24 1221.80 249.30 o 13 0 0 106.55 488.08 244.56 o -13 1 0 11.84 86.55 284.24 o -12 1 0 785.25 898.64 174.23 o -11 1 0 326.47 261.48 182.00 o -10 1 0 1027.15 1120.93 151.66 o -9 1 0 718.42 786.55 134.89 o -8 1 0 2654.53 2555.32 153.39 o -7 1 0 13491.91 13030.60 411.56 o -6 1 0 11973.83 12317.46 345.72 o -5 1 0 4083.53 4267.28 86.45 o -4 1 0 3419.40 3408.55 64.95 o -3 1 0 24620.15 25719.61 130.46 o -2 1 0 9673.38 10325.30 89.09 o -1 1 0 17944.54 17581.45 346.31 o 2 1 0 2556.63 2825.87 36.41 o 3 1 0 680.59 682.22 26.67 o 4 1 0 2230.14 2182.12 81.65 o 5 1 0 144145.53 141409.77 2192.06 o 6 1 0 653.20 635.15 45.61 o 7 1 0 14.78 -8.85 48.12 o 8 1 0 1325.55 1289.55 115.43 o 9 1 0 2275.54 2362.37 138.92 o 10 1 0 278.70 410.69 143.02 o 11 1 0 686.34 741.08 155.50 o 12 1 0 0.52 108.19 247.42 o 13 1 0 39.18 264.43 290.24 o -12 2 0 20.29 122.98 175.77 o -11 2 0 1083.68 1211.95 180.36 o -10 2 0 436.23 634.41 199.48 o -9 2 0 1544.02 1643.08 141.98 o -8 2 0 780.83 867.48 112.11 o -7 2 0 18901.16 18858.98 375.23 o -6 2 0 194.74 194.16 78.83 o -5 2 0 9108.75 9064.24 108.73 o -4 2 0 1693.69 1675.11 96.68 o -3 2 0 23697.81 22919.62 174.68 o -2 2 0 27102.91 25460.38 169.29 o -1 2 0 41389.56 38758.00 164.29 o 0 2 0 16074.03 17022.31 66.76 o 1 2 0 685.53 1165.65 50.17 o 2 2 0 81.18 146.54 27.85 o 3 2 0 63.09 174.32 25.39 o 4 2 0 4041.48 4609.68 78.72 o 5 2 0 2806.04 2865.84 179.83 o 6 2 0 3554.47 3341.35 120.33 o 7 2 0 1112.72 1206.20 72.03 o 8 2 0 1262.62 1234.52 72.29 o 9 2 0 2524.25 2782.26 138.78 o 10 2 0 5733.23 6429.22 173.33 o 11 2 0 14.83 218.80 235.97 o 12 2 0 80.35 72.34 269.12 o 13 2 0 132.57 97.95 302.18 o -12 3 0 2.98 59.19 188.72 o -11 3 0 1.68 28.06 175.45 o -10 3 0 654.35 686.24 152.56 o -9 3 0 14.07 25.19 132.42 o -8 3 0 3075.10 3493.94 134.12 o -7 3 0 355.43 442.95 105.84 o -6 3 0 14242.01 14082.98 162.79 o -5 3 0 1810.13 1783.61 119.99 o -4 3 0 2798.87 2766.57 115.35 o -3 3 0 13482.28 13782.00 111.49 o -2 3 0 67609.02 61964.93 802.27 o -1 3 0 5694.22 5603.18 98.15 o 0 3 0 179.61 335.80 65.61 o 1 3 0 3573.29 3889.93 40.92 o 2 3 0 19759.19 21660.00 137.94 o 3 3 0 910.35 953.39 59.93 o 4 3 0 3655.43 4160.86 139.14 o 5 3 0 6398.77 6947.79 221.56 o 6 3 0 1417.50 1326.35 94.57 o 7 3 0 51.50 98.04 68.13 o 8 3 0 923.63 974.64 74.10 o 9 3 0 1769.37 2065.42 189.51 o 10 3 0 427.39 605.18 198.66 o 11 3 0 18.51 38.51 245.29 o 12 3 0 378.97 400.68 250.22 o 13 3 0 130.97 182.55 304.17 o -12 4 0 68.14 21.14 170.40 o -11 4 0 235.13 362.66 166.02 o -10 4 0 1029.53 1067.79 160.41 o -9 4 0 329.13 384.69 135.75 o -8 4 0 97.17 53.29 59.65 o -7 4 0 1139.89 1061.93 81.45 o -6 4 0 216.12 189.90 145.94 o -5 4 0 2603.81 2885.93 146.48 o -4 4 0 108.75 149.98 62.92 o -3 4 0 12316.81 12371.14 183.73 o -2 4 0 7970.85 7754.28 57.33 o -1 4 0 34264.71 32603.48 374.17 o 0 4 0 705.32 928.20 58.74 o 1 4 0 2311.59 2180.57 95.91 o 2 4 0 37720.88 39059.88 239.61 o 3 4 0 35082.23 35217.15 303.89 o 4 4 0 6567.34 7070.36 103.83 o 5 4 0 291.34 223.61 56.30 o 6 4 0 49.33 14.60 72.23 o 7 4 0 2612.08 2353.02 140.72 o 8 4 0 1476.14 1292.57 96.21 o 9 4 0 11.65 -5.42 91.57 o 10 4 0 413.86 434.85 223.15 o 11 4 0 9.14 -8.10 234.76 o 12 4 0 0.63 -10.95 280.33 o 13 4 0 67.91 281.82 288.39 o -11 5 0 154.90 182.37 169.08 o -10 5 0 50.01 -7.59 153.90 o -9 5 0 2880.23 2868.58 203.20 o -8 5 0 11.12 31.98 66.22 o -7 5 0 99.54 122.83 60.23 o -6 5 0 4196.22 3822.58 160.09 o -5 5 0 13110.11 12109.86 363.14 o -4 5 0 1249.24 953.41 120.77 o -3 5 0 4218.41 3916.82 112.48 o -2 5 0 5732.38 5588.66 124.81 o -1 5 0 4282.17 4502.34 84.70 o 0 5 0 183.92 211.15 41.45 o 1 5 0 13.97 22.20 27.89 o 2 5 0 17145.54 16819.94 88.63 o 3 5 0 7256.52 7469.35 63.84 o 4 5 0 5328.05 5708.49 70.32 o 5 5 0 11901.66 12658.18 161.81 o 6 5 0 457.04 412.32 64.87 o 7 5 0 5662.48 5595.37 349.31 o 8 5 0 2732.24 2906.65 266.89 o 9 5 0 14.50 -53.79 104.25 o 10 5 0 196.66 256.68 236.35 o 11 5 0 86.50 139.89 231.07 o 12 5 0 0.33 -23.93 250.84 o 13 5 0 180.58 184.15 264.15 o -11 6 0 10.97 1.07 178.75 o -10 6 0 1.25 86.98 153.61 o -9 6 0 51.87 -42.72 98.26 o -8 6 0 1620.43 1479.51 89.30 o -7 6 0 77.50 52.77 80.01 o -6 6 0 410.21 368.31 67.05 o -5 6 0 473.71 479.67 59.75 o -4 6 0 12876.78 11865.43 309.29 o -3 6 0 4575.79 4138.00 160.38 o -2 6 0 10149.31 9084.03 90.88 o -1 6 0 24951.96 23292.22 217.23 o 0 6 0 12699.15 13606.87 106.76 o 1 6 0 3587.51 3829.19 125.91 o 2 6 0 27142.21 27254.04 124.08 o 3 6 0 2622.76 2720.93 96.16 o 4 6 0 13799.26 13234.72 138.27 o 5 6 0 12.91 21.60 57.52 o 6 6 0 18.11 70.34 68.06 o 7 6 0 1083.64 1168.64 85.64 o 8 6 0 303.87 189.64 115.39 o 9 6 0 32.51 6.29 112.84 o 10 6 0 1201.20 1191.89 125.15 o 11 6 0 3.65 -185.69 237.00 o 12 6 0 1048.80 1386.13 315.28 o 13 6 0 90.24 71.81 330.47 o -10 7 0 0.45 13.99 156.28 o -9 7 0 489.69 354.75 89.54 o -8 7 0 74.50 38.95 83.05 o -7 7 0 772.49 700.94 137.63 o -6 7 0 3.79 58.86 78.97 o -5 7 0 795.69 633.10 64.28 o -4 7 0 93.34 55.00 59.72 o -3 7 0 2365.82 2058.68 68.11 o -2 7 0 1386.47 1242.76 62.50 o -1 7 0 1190.32 1117.22 60.80 o 0 7 0 2031.70 1871.65 53.34 o 1 7 0 5829.43 5665.64 127.56 o 2 7 0 3808.75 3885.02 94.26 o 3 7 0 14091.69 13551.63 379.87 o 4 7 0 12866.91 12478.33 236.20 o 5 7 0 989.57 1050.33 64.62 o 6 7 0 788.88 820.89 83.33 o 7 7 0 5029.50 5203.55 224.67 o 8 7 0 1346.13 1374.84 351.33 o 9 7 0 2138.70 2122.56 145.01 o 10 7 0 32.79 5.35 134.82 o 11 7 0 115.60 -29.08 245.35 o 12 7 0 35.52 73.41 288.54 o 13 7 0 24.56 109.58 326.29 o -10 8 0 9.48 -179.25 179.25 o -9 8 0 146.19 187.17 96.00 o -8 8 0 898.82 641.70 113.02 o -7 8 0 294.25 251.70 97.25 o -6 8 0 30.31 46.13 73.58 o -5 8 0 1147.76 1027.47 75.34 o -4 8 0 1831.01 1624.87 73.68 o -3 8 0 427.37 339.52 46.81 o -2 8 0 106.60 36.92 48.46 o -1 8 0 1393.13 1275.90 68.55 o 0 8 0 1028.19 1009.88 54.33 o 1 8 0 351.05 387.64 52.66 o 2 8 0 13.92 30.78 45.78 o 3 8 0 7281.31 6816.82 346.41 o 4 8 0 3783.07 3711.64 108.83 o 5 8 0 10141.24 10019.93 264.58 o 6 8 0 2.56 -12.30 84.91 o 7 8 0 714.01 607.44 122.05 o 8 8 0 565.75 404.92 141.04 o 9 8 0 2529.45 2564.92 339.54 o 10 8 0 40.66 15.81 142.71 o 11 8 0 107.56 90.36 253.18 o 12 8 0 111.80 78.58 260.23 o 13 8 0 270.42 665.13 317.26 o -9 9 0 117.96 112.92 111.09 o -8 9 0 19.94 -112.70 112.70 o -7 9 0 1110.68 796.52 107.64 o -6 9 0 494.90 443.19 83.08 o -5 9 0 789.58 751.03 79.32 o -4 9 0 8183.34 7276.01 119.56 o -3 9 0 1217.86 1063.45 90.12 o -2 9 0 2811.65 2307.54 91.69 o -1 9 0 2399.41 2121.08 122.33 o 0 9 0 6278.07 5960.69 111.39 o 1 9 0 41.80 91.21 54.98 o 2 9 0 83.47 106.41 66.02 o 3 9 0 2055.58 1929.81 71.51 o 4 9 0 2168.15 2083.90 73.51 o 5 9 0 241.83 214.46 70.84 o 6 9 0 2121.02 1947.98 179.59 o 7 9 0 17.48 -107.57 121.94 o 8 9 0 1166.34 1114.09 188.01 o 9 9 0 809.04 781.23 154.92 o 10 9 0 3684.05 3733.09 451.79 o 11 9 0 171.29 174.01 151.29 o 12 9 0 105.80 95.74 335.35 o 13 9 0 24.80 -16.81 349.69 o -9 10 0 88.07 -37.85 139.77 o -8 10 0 5.52 -95.90 161.00 o -7 10 0 104.70 48.52 147.94 o -6 10 0 27.60 68.94 92.30 o -5 10 0 587.07 587.74 89.32 o -4 10 0 1751.96 1549.24 85.18 o -3 10 0 560.30 476.98 76.96 o -2 10 0 3976.53 3515.56 75.72 o -1 10 0 509.95 457.50 56.03 o 0 10 0 851.29 831.29 53.95 o 1 10 0 19411.84 18493.37 156.69 o 2 10 0 1373.97 1467.34 58.96 o 3 10 0 5808.07 5390.55 158.17 o 4 10 0 5144.12 4769.74 131.75 o 5 10 0 2341.04 2055.78 174.17 o 6 10 0 90.83 9.14 159.83 o 7 10 0 362.56 290.70 180.69 o 8 10 0 844.59 627.06 177.11 o 9 10 0 0.49 -150.19 152.49 o 10 10 0 8.55 -59.26 165.22 o 11 10 0 344.48 301.98 159.17 o 12 10 0 18.29 -175.43 297.81 o -8 11 0 12.69 -105.14 181.47 o -7 11 0 246.50 185.24 169.75 o -6 11 0 696.84 528.42 129.45 o -5 11 0 46.34 -30.46 123.46 o -4 11 0 903.21 959.61 111.27 o -3 11 0 41.19 30.63 112.87 o -2 11 0 32.51 -104.46 104.46 o -1 11 0 103.16 -22.39 76.49 o 0 11 0 935.10 856.18 76.73 o 1 11 0 5049.58 5159.98 89.93 o 2 11 0 265.04 288.94 63.61 o 3 11 0 7484.53 7307.06 136.06 o 4 11 0 58.98 224.78 64.31 o 5 11 0 775.07 781.13 97.11 o 6 11 0 4569.71 4473.01 224.25 o 7 11 0 3218.65 3127.91 210.21 o 8 11 0 707.32 505.94 201.45 o 9 11 0 1762.36 1421.86 198.02 o 10 11 0 290.88 59.17 189.38 o 11 11 0 25.06 -182.25 182.25 o 12 11 0 198.98 55.28 170.79 o -7 12 0 98.25 -108.98 185.61 o -6 12 0 261.55 255.48 142.56 o -5 12 0 1365.20 1281.55 141.09 o -4 12 0 39.53 -39.99 122.27 o -3 12 0 399.71 355.21 103.62 o -2 12 0 2049.49 1973.41 119.10 o -1 12 0 843.80 745.05 83.37 o 0 12 0 12.04 -28.66 82.90 o 1 12 0 941.09 856.96 80.78 o 2 12 0 839.11 751.94 92.23 o 3 12 0 4.20 29.34 69.33 o 4 12 0 814.93 799.53 101.16 o 5 12 0 16.32 -70.37 103.97 o 6 12 0 2129.06 2012.98 220.53 o 7 12 0 28.63 120.87 215.92 o 8 12 0 4064.66 4170.42 255.45 o 9 12 0 277.48 149.96 204.08 o 10 12 0 124.35 80.96 192.16 o 11 12 0 385.40 258.57 200.82 o 12 12 0 825.04 781.36 250.86 o -6 13 0 168.27 65.49 153.28 o -5 13 0 79.98 -3.01 129.48 o -4 13 0 1532.09 1596.54 128.40 o -3 13 0 49.65 78.30 114.16 o -2 13 0 628.56 696.23 105.23 o -1 13 0 546.58 484.43 113.65 o 0 13 0 4528.96 4459.23 143.89 o 1 13 0 12.77 -40.89 86.65 o 2 13 0 1820.02 1848.74 91.81 o 3 13 0 2190.59 2408.78 125.02 o 4 13 0 178.61 200.78 97.50 o 5 13 0 75.12 80.80 118.42 o 6 13 0 9.17 48.48 214.72 o 7 13 0 540.90 664.34 227.85 o 8 13 0 135.45 171.97 235.46 o 9 13 0 238.69 159.69 236.75 o 10 13 0 103.80 14.07 224.33 o 11 13 0 302.21 182.82 210.51 o -5 14 0 37.00 -121.20 127.87 o -4 14 0 88.73 19.64 131.13 o -3 14 0 348.26 353.67 120.97 o -2 14 0 1.04 29.52 115.00 o -1 14 0 470.10 372.92 127.63 o 0 14 0 3.73 20.30 94.06 o 1 14 0 5114.62 5443.39 153.99 o 2 14 0 8.20 -59.47 118.73 o 3 14 0 776.99 736.24 114.45 o 4 14 0 714.72 713.81 107.78 o 5 14 0 3732.00 3575.11 215.95 o 6 14 0 299.92 389.41 209.29 o 7 14 0 1027.58 767.53 247.83 o 8 14 0 527.62 541.33 226.90 o 9 14 0 7.63 -143.47 237.37 o 10 14 0 2.99 -96.41 254.04 o -4 15 0 188.30 124.32 128.47 o -3 15 0 46.09 65.85 131.89 o -2 15 0 493.01 458.35 122.94 o -1 15 0 178.27 180.44 126.73 o 0 15 0 126.70 149.34 121.85 o 1 15 0 130.49 201.99 127.94 o 2 15 0 230.36 167.03 126.40 o 3 15 0 116.16 8.74 129.44 o 4 15 0 735.32 665.40 121.06 o 5 15 0 60.36 131.05 140.42 o 6 15 0 3272.23 3459.38 278.76 o 7 15 0 223.59 116.49 260.92 o 8 15 0 64.01 142.91 237.09 o 9 15 0 385.32 438.14 229.73 o -3 16 0 431.15 486.84 148.71 o -2 16 0 246.04 244.09 128.40 o -1 16 0 11.61 41.52 146.56 o 0 16 0 41.28 15.83 196.48 o 1 16 0 482.52 672.85 149.40 o 2 16 0 50.33 105.59 137.49 o 3 16 0 251.42 179.50 135.66 o 4 16 0 388.96 275.49 128.75 o 5 16 0 34.01 -10.91 215.69 o 6 16 0 50.96 -42.12 247.53 o 7 16 0 0.54 -8.45 227.03 o 8 16 0 62.60 263.43 273.16 o -1 17 0 531.61 601.16 176.95 o 0 17 0 375.16 458.60 220.27 o 1 17 0 88.76 167.65 212.74 o 2 17 0 620.06 761.02 154.82 o 3 17 0 292.14 316.87 139.61 o 4 17 0 106.44 124.09 139.92 o 5 17 0 0.05 213.32 247.21 o 6 17 0 383.60 243.59 288.09 o 3 18 0 376.98 405.07 146.77 o 4 18 0 312.48 490.64 151.80 o -6 -17 1 13.34 76.77 285.02 o -5 -17 1 349.03 373.85 230.71 o -4 -17 1 75.57 4.89 122.80 o -3 -17 1 438.27 365.19 145.59 o -2 -17 1 346.01 374.96 142.51 o -1 -17 1 534.29 409.99 210.47 o 0 -17 1 301.07 266.23 209.07 o -7 -16 1 24.06 -54.67 214.53 o -6 -16 1 40.01 38.53 215.03 o -5 -16 1 118.30 182.40 266.64 o -4 -16 1 541.95 429.45 118.19 o -3 -16 1 153.21 167.60 134.03 o -2 -16 1 53.58 65.59 131.24 o -1 -16 1 1.76 -70.66 187.76 o 0 -16 1 229.27 164.50 192.80 o 1 -16 1 116.98 156.95 151.34 o 2 -16 1 320.79 332.81 134.77 o -9 -15 1 137.80 89.48 212.79 o -8 -15 1 439.75 427.01 256.62 o -7 -15 1 585.98 551.67 248.39 o -6 -15 1 182.49 76.76 255.03 o -5 -15 1 838.91 726.56 232.33 o -4 -15 1 639.81 729.58 117.43 o -3 -15 1 804.33 792.37 126.29 o -2 -15 1 54.39 18.20 121.73 o -1 -15 1 15.76 -36.35 125.94 o 0 -15 1 126.04 176.97 123.95 o 1 -15 1 669.25 672.16 131.93 o 2 -15 1 8.76 18.66 120.17 o 3 -15 1 118.72 40.47 135.24 o 4 -15 1 7.10 43.81 135.71 o -10 -14 1 194.15 176.61 267.17 o -9 -14 1 81.50 123.04 252.91 o -8 -14 1 2.31 -107.31 249.36 o -7 -14 1 1436.34 1893.29 257.21 o -6 -14 1 2391.18 2632.62 266.01 o -5 -14 1 63.59 120.51 238.60 o -4 -14 1 476.26 384.62 105.90 o -3 -14 1 463.36 421.25 112.73 o -2 -14 1 993.65 907.33 118.23 o -1 -14 1 145.25 195.79 93.43 o 0 -14 1 501.39 392.81 98.76 o 1 -14 1 188.76 171.83 120.60 o 2 -14 1 537.21 618.41 120.00 o 3 -14 1 44.86 -26.84 117.60 o 4 -14 1 1.19 -63.59 130.55 o 5 -14 1 7.03 -72.24 136.99 o -11 -13 1 4.73 7.02 216.13 o -10 -13 1 85.33 111.24 223.48 o -9 -13 1 114.81 -50.98 230.71 o -8 -13 1 41.88 68.91 242.15 o -7 -13 1 8.88 4.07 224.53 o -6 -13 1 105.97 117.22 218.36 o -5 -13 1 306.30 164.83 190.97 o -4 -13 1 1213.85 1061.21 103.33 o -3 -13 1 234.09 187.12 99.39 o -2 -13 1 1289.70 1297.26 90.61 o -1 -13 1 2259.82 2136.31 94.38 o 0 -13 1 135.95 86.11 86.51 o 1 -13 1 615.42 639.19 113.18 o 2 -13 1 108.50 93.79 103.38 o 3 -13 1 266.34 259.19 113.16 o 4 -13 1 203.08 110.17 119.45 o 5 -13 1 343.73 284.04 131.04 o 6 -13 1 0.04 -141.77 141.77 o -11 -12 1 141.45 220.52 203.21 o -10 -12 1 699.95 507.87 200.62 o -9 -12 1 176.89 -45.78 233.90 o -8 -12 1 17.67 -86.42 195.24 o -7 -12 1 3023.42 2986.14 223.03 o -6 -12 1 17.13 120.15 206.24 o -5 -12 1 1430.88 1295.03 187.26 o -4 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