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Acta Cryst. (2013). E69, m353  [ doi:10.1107/S1600536813014335 ]

Tris(N,N-dimethylanilinium) tri-[mu]-bromido-bis[tribromidoantimonate(III)]

H. Kharrat, S. Kamoun and F. Michaud


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT213_ALERT_2_B Atom C20A has ADP max/min Ratio ..... 4.5 prola PLAT213_ALERT_2_B Atom C20B has ADP max/min Ratio ..... 4.5 prola PLAT234_ALERT_4_B Large Hirshfeld Difference C12A -- C13A .. 0.29 Ang. PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 12
Alert level C PLAT213_ALERT_2_C Atom C17A has ADP max/min Ratio ..... 3.1 prola PLAT213_ALERT_2_C Atom C18A has ADP max/min Ratio ..... 3.1 prola PLAT213_ALERT_2_C Atom C17B has ADP max/min Ratio ..... 3.1 prola PLAT213_ALERT_2_C Atom C18B has ADP max/min Ratio ..... 3.1 prola PLAT234_ALERT_4_C Large Hirshfeld Difference C4 -- C5 .. 0.17 Ang. PLAT234_ALERT_4_C Large Hirshfeld Difference N2A -- C16A .. 0.16 Ang. PLAT234_ALERT_4_C Large Hirshfeld Difference C13A -- C14A .. 0.22 Ang. PLAT234_ALERT_4_C Large Hirshfeld Difference C17A -- C18A .. 0.18 Ang. PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Sb1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Sb2 PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.3 PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.3 PLAT331_ALERT_2_C Small Average Phenyl C-C Dist. C1 -C6 1.36 Ang. PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0113 Ang PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.603 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 5
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 36 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined Donor-H Atoms ........ 5 PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C14A PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C17A PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C14B PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C17B PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 47 % PLAT794_ALERT_5_G Note: Tentative Bond Valency for Sb1 (III) 2.85 PLAT794_ALERT_5_G Note: Tentative Bond Valency for Sb2 (III) 2.97 PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... ! PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 88 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 156
0 ALERT level A = Most likely a serious problem - resolve or explain 4 ALERT level B = A potentially serious problem, consider carefully 16 ALERT level C = Check. Ensure it is not caused by an omission or oversight 14 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 16 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 6 ALERT type 4 Improvement, methodology, query or suggestion 5 ALERT type 5 Informative message, check

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