[HTML version][PDF version][Article Abstract][CIF][3d view][Structure Factors][Supplementary Material][Issue contents]  [Open access]

Acta Cryst. (2013). E69, i41  [ doi:10.1107/S1600536813016620 ]

Redetermination of katayamalite, KLi3Ca7Ti2(SiO3)12(OH)2

M. B. Andrade, D. Doell, R. T. Downs and H. Yang


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT420_ALERT_2_B D-H Without Acceptor O19 - H1 ... ? Check
Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.961 PLAT354_ALERT_3_C Short O-H (X0.82,N0.98A) O19 - H1 ... 0.68 Ang. PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 103
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 2 PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 2 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT793_ALERT_4_G The Model has Chirality at Si1 (Verify) .... S PLAT793_ALERT_4_G The Model has Chirality at Si2 (Verify) .... S PLAT793_ALERT_4_G The Model has Chirality at Si3 (Verify) .... R PLAT793_ALERT_4_G The Model has Chirality at Si4 (Verify) .... S PLAT793_ALERT_4_G The Model has Chirality at Si5 (Verify) .... R PLAT793_ALERT_4_G The Model has Chirality at Si6 (Verify) .... R PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 1 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 601 PLAT952_ALERT_5_G Reported and Calculated Lmax Values Differ by .. 4
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 14 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 7 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster