Acta Crystallographica Section E

Structure Reports Online

Volume 69, Part 8 (August 2013)


organic compounds



gw2136 scheme

Acta Cryst. (2013). E69, o1282    [ doi:10.1107/S1600536813019211 ]

2-(10',10'-Dimethyl-3'-sulfanylidene-4'-azatricyclo[5.2.1.01,5]decan-2'-yl)-10,10-dimethyl-4-azatricyclo[5.2.1.01,5]decane-3-thione

A. Walker, C. M. Forsyth and P. Perlmutter

Abstract: The title compound, C28H40N2O2S2, was obtained as a minor product from an anti-aldol reaction between the corresponding N-propionylthiolactam and benzaldehyde. The asymmetric unit contains one half-molecule, which is completed by inversion symmetry. The molecule displays a nearly eclipsed conformation along the central C-C bond with a C-C-C-C- torsion angle of 20.4 (3)°.


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