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Acta Cryst. (2013). E69, m428  [ doi:10.1107/S1600536813015493 ]

Bis(1-ethyl-4,4'-bipyridin-1-ium) bis(1,2-dicyanoethene-1,2-dithiolato-[kappa]2S,S')nickelate(II)

Y. Chen, W. Ning and J.-L. Liu


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Alert level C PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low .... 47 % PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.970 PLAT230_ALERT_2_C Hirshfeld Test Diff for C19 -- C20 .. 6.4 su PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for S4 PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.1 PLAT341_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0062 Ang PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 4.273 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 48
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00200 Deg. PLAT371_ALERT_2_G Long C(sp2)-C(sp1) Bond C1 - C2 ... 1.43 Ang. PLAT371_ALERT_2_G Long C(sp2)-C(sp1) Bond C3 - C4 ... 1.42 Ang. PLAT371_ALERT_2_G Long C(sp2)-C(sp1) Bond C5 - C6 ... 1.44 Ang. PLAT371_ALERT_2_G Long C(sp2)-C(sp1) Bond C7 - C8 ... 1.43 Ang. PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 185
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 9 ALERT level C = Check. Ensure it is not caused by an omission or oversight 7 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 7 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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