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Acta Cryst. (2013). E69, m457  [ doi:10.1107/S1600536813019259 ]

Bis{N-benzyl-N-[2-(thiophen-2-yl)ethyl]dithiocarbamato-[kappa]2S,S'}lead(II)

E. Sathiyaraj, S. Thirumaran, B. Sridhar and S. Selvanayagam


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT741_ALERT_1_C Bond Calc 1.390(2), Rep 1.39000 ...... Missing su C9 -C10 1.555 1.555 # 36 PLAT741_ALERT_1_C Bond Calc 1.390(3), Rep 1.39000 ...... Missing su C9 -C14 1.555 1.555 # 37 PLAT741_ALERT_1_C Bond Calc 1.390(3), Rep 1.39000 ...... Missing su C10 -C11 1.555 1.555 # 38 PLAT741_ALERT_1_C Bond Calc 1.390(3), Rep 1.39000 ...... Missing su C11 -C12 1.555 1.555 # 40 PLAT741_ALERT_1_C Bond Calc 1.390(3), Rep 1.39000 ...... Missing su C12 -C13 1.555 1.555 # 42 PLAT741_ALERT_1_C Bond Calc 1.390(3), Rep 1.39000 ...... Missing su C13 -C14 1.555 1.555 # 44 PLAT742_ALERT_1_C Angle Calc 119.99(15), Rep 120.00 ...... Missing su C10 -C9 -C14 1.555 1.555 1.555 # 60 PLAT742_ALERT_1_C Angle Calc 120.02(17), Rep 120.00 ...... Missing su C11 -C10 -C9 1.555 1.555 1.555 # 63 PLAT742_ALERT_1_C Angle Calc 120.00(16), Rep 120.00 ...... Missing su C12 -C11 -C10 1.555 1.555 1.555 # 66 PLAT742_ALERT_1_C Angle Calc 119.99(17), Rep 120.00 ...... Missing su C11 -C12 -C13 1.555 1.555 1.555 # 69 PLAT742_ALERT_1_C Angle Calc 120.02(18), Rep 120.00 ...... Missing su C14 -C13 -C12 1.555 1.555 1.555 # 72 PLAT742_ALERT_1_C Angle Calc 120.00(15), Rep 120.00 ...... Missing su C13 -C14 -C9 1.555 1.555 1.555 # 75 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT230_ALERT_2_G Hirshfeld Test Diff for S3 -- C4 .. 10.0 su PLAT230_ALERT_2_G Hirshfeld Test Diff for C4 -- C5 .. 8.5 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Pb1 -- S2 .. 7.8 su PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C4 PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C4' PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 27 % PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... ! Info PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 23 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 49
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 13 ALERT level C = Check. Ensure it is not caused by an omission or oversight 10 ALERT level G = General information/check it is not something unexpected 12 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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