[HTML version][PDF version][Article Abstract][CIF][3d view][Structure Factors][Supplementary Material][Issue contents]  [Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o1229  [ doi:10.1107/S1600536813018576 ]

5-Fluoro-N-(2-methyl-3-oxo-1-thia-4-azaspiro[4.5]dec-4-yl)-3-phenyl-1H-indole-2-carboxamide

S. T. Çelikesir, M. Akkurt, G. C. Üstündag and O. Büyükgüngör


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.9 Ratio PLAT222_ALERT_3_C Large Non-Solvent H Uiso(max)/Uiso(min) .. 4.1 Ratio PLAT230_ALERT_2_C Hirshfeld Test Diff for O2 -- C16 .. 6.0 su PLAT230_ALERT_2_C Hirshfeld Test Diff for N3 -- C16 .. 7.0 su PLAT230_ALERT_2_C Hirshfeld Test Diff for C9 -- C10 .. 5.3 su PLAT230_ALERT_2_C Hirshfeld Test Diff for C10 -- C11 .. 5.5 su PLAT230_ALERT_2_C Hirshfeld Test Diff for C17 -- C18 .. 6.7 su PLAT230_ALERT_2_C Hirshfeld Test Diff for C22 -- C23 .. 5.2 su PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C17 PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0051 Ang. PLAT360_ALERT_2_C Short C(sp3)-C(sp3) Bond C17 - C18 ... 1.35 Ang. PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of . 57 Ang3 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 5.960 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.148
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 6 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size .... 0.68 mm PLAT791_ALERT_4_G Note: The Model has Chirality at C17 (Verify) S PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 4
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 14 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 11 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster