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Acta Cryst. (2013). E69, o1328-o1329  [ doi:10.1107/S1600536813020485 ]

1-Ethyl-4'-(1H-indol-3-ylcarbonyl)-1'-methyl-2,2''-dioxodispiro[indoline-3,2'-pyrrolidine-3',3''-indoline]-4'-carbonitrile dimethyl sulfoxide monosolvate

S. A. Inglebert, Y. Arun, K. Sethusankar and P. T. Perumal


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Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.976 PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.3 PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -3.288 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 3 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 124
Alert level G PLAT003_ALERT_2_G Number of Uiso or Uij Restrained non-H Atoms ... 6 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of S1 PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 75 % PLAT793_ALERT_4_G The Model has Chirality at C10 (Verify) .... S PLAT793_ALERT_4_G The Model has Chirality at C13 (Verify) .... R PLAT793_ALERT_4_G The Model has Chirality at C14 (Verify) .... R PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 48 PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 40 %
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 9 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 5 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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