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Acta Cryst. (2013). E69, m446-m447  [ doi:10.1107/S1600536813017376 ]

Dichloridobis[3-(4-chlorophenyl)-2,N,N-trimethyl-2,3-dihydro-1,2,4-oxadiazole-5-amine-[kappa]N4]platinum(II)-4-chlorobenzaldehyde (1/1)

A. S. Kritchenkov, V. V. Gurzhiy, N. A. Bokach and V. A. Kalibabchuk


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.4 PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 3.4 PLAT420_ALERT_2_C D-H Without Acceptor N2 - H2 ... ? Check PLAT715_ALERT_1_C D-H Unknown or Inconsistent Label .......... H8 C8 H8 PLAT716_ALERT_1_C H...A Unknown or Inconsistent Label .......... H8 H8 O2 PLAT718_ALERT_1_C D-H..A Unknown or Inconsistent Label .......... H8 C8 H8 O2 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 2 PLAT971_ALERT_2_C Large Calcd. Non-Metal Positive Residual Density 1.57 eA-3 PLAT976_ALERT_2_C Negative Residual Density at 1.09A from N2 . -0.47 eA-3
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT007_ALERT_5_G Note: Number of Unrefined Donor-H Atoms ........ 1 PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 33 % PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 17 N4 -PT1 -N4 -C3 15.00 24.00 2.665 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 18 N4 -PT1 -N4 -C5 -155.00 24.00 2.665 1.555 1.555 1.555 PLAT779_ALERT_4_G Suspect or Irrelevant (Bond) Angle in CIF .... # 73 C21 -C20 -CL21 1.555 1.555 1.555 11.60 Deg. PLAT793_ALERT_4_G The Model has Chirality at N2 (Verify) .... S PLAT793_ALERT_4_G The Model has Chirality at C3 (Verify) .... S PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... ! Check
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 9 ALERT level C = Check. Ensure it is not caused by an omission or oversight 9 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 6 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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