Acta Crystallographica Section E

Structure Reports Online

Volume 69, Part 8 (August 2013)


organic compounds



sj5340 scheme

Acta Cryst. (2013). E69, o1232    [ doi:10.1107/S1600536813018539 ]

N-(3-Methoxybenzoyl)-2-methylbenzenesulfonamide

S. Sreenivasa, D. Darshan, M. Prakash Shet, N. R. Mohan, V. Kumar and P. A. Suchetan

Abstract: In the title compound, C15H15NO4S, the dihedral angle between the methyl- and methoxy-substituted benzene rings is 88.99 (12)°. An intramolecular C-H...O hydrogen bond occurs. In the crystal, adjacent molecules form inversion-related dimers through strong N-H...O hydrogen bonds, generating R22(8) loops. The dimers are further connected through C-H...O interactions that form C(8) chains parallel to (001). Molecules are also connected through other C-H...O hydrogen bonds along the b axis, forming additional C(8) chains. Two aromatic [pi]-[pi] stacking interactions [centroid-centroid separations = 3.6150 (1) and 3.6837 (1) Å] generate a three-dimensional architecture.


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