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Acta Cryst. (2013). E69, o1211-o1212  [ doi:10.1107/S1600536813018436 ]

5-Fluoro-N'-(4-methylcyclohexylidene)-3-phenyl-1H-indole-2-carbohydrazide

S. T. Çelikesir, M. Akkurt, G. C. Üstündag, G. Çapan and O. Büyükgüngör


Key indicators

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Alert level C PLAT019_ALERT_1_C Check _diffrn_measured_fraction_theta_full/_max 0.997 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C41 PLAT414_ALERT_2_C Short Intra D-H..H-X H2N .. H17B .. 1.98 Ang. PLAT420_ALERT_2_C D-H Without Acceptor N2 - H2N ... ? Check PLAT420_ALERT_2_C D-H Without Acceptor N5 - H5N ... ? Check PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 13.133 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.950 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 3 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 51
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT007_ALERT_5_G Note: Number of Unrefined Donor-H Atoms ........ 2 PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size .... 0.68 mm PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00400 Deg. PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 2 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 158
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 9 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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