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Acta Cryst. (2013). E69, m472  [ doi:10.1107/S1600536813019806 ]

trans-Bis([mu]-benzenethiolato-[kappa]2S:S)bis[chlorido(triphenylphosphane-[kappa]P)palladium(II)] chloroform disolvate

A. Avila-Sorrosa, A. Reyes-Arellano, J. M. Germán-Acacio, R. Reyes-Martínez and D. Morales-Morales


Key indicators

checkCIF/PLATON results

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Alert level C PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C3 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C1 PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C25 PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0085 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H15 .. CL1 .. 2.93 Ang. PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 6
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT128_ALERT_4_G Note: Alternate Setting of Space-group P21/c . P21/n PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Pd1 -- S1_a .. 6.0 su PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 75 % PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 96 PLAT870_ALERT_4_G ALERTS Related to Twinning Effects Suppressed .. ! Info PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 19 PLAT931_ALERT_5_G Check Twin Law ( 0 0 1)[ ] Estimated BASF 0.24
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 8 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 6 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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