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Acta Cryst. (2013). E69, m473-m474  [ doi:10.1107/S1600536813019284 ]

Bis(cyclohexylammonium) tetrachlorido(oxalato)stannate(IV)

M. Sarr, A. Diasse-Sarr, W. Diallo, L. Plasseraud and H. Cattey


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Alert level B PLAT029_ALERT_3_B _diffrn_measured_fraction_theta_full Low ....... 0.957
Author Response: Several crystals have been attempted but unfortunately, these crystals did not diffract too much

Alert level C PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.326 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 4 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 115
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT007_ALERT_5_G Note: Number of Unrefined Donor-H Atoms ........ 6 PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? Check PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 5.70 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 107
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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