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Acta Cryst. (2013). E69, m431-m432  [ doi:10.1107/S1600536813017881 ]

Tetrakis([mu]-3-chlorobenzoato-[kappa]2O:O')bis[(N,N-diethylnicotinamide-[kappa]N1)copper(II)]

N. Bozkurt, T. Tunç, N. Çaylak Delibas, H. Necefoglu and T. Hökelek


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Alert level C PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.3 Ratio PLAT918_ALERT_3_C Reflection(s) # with I(obs) much smaller I(calc) 1
Alert level G PLAT003_ALERT_2_G Number of Uiso or Uij Restrained non-H Atoms ... 34 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 85 PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... ! Check
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 2 ALERT level C = Check. Ensure it is not caused by an omission or oversight 4 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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