# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title '101116_s1_zlk in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 323.08 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.8000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.4260 _cell_length_b 12.9136 _cell_length_c 17.9749 _cell_angle_alpha 89.753 _cell_angle_beta 79.447 _cell_angle_gamma 71.298 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 158.92 181.84 12.60 o 3 0 0 20775.63 21727.18 252.78 o 4 0 0 8456.16 8469.65 103.93 o 5 0 0 4639.80 4621.71 76.09 o 6 0 0 6563.49 6631.50 99.22 o 7 0 0 17.46 27.77 13.79 o 8 0 0 6821.54 6753.78 134.17 o 9 0 0 10485.33 10572.20 230.97 o 10 0 0 5042.91 4884.53 158.01 o 11 0 0 85.49 52.37 35.38 o 12 0 0 2171.77 2366.80 214.12 o 13 0 0 1457.74 1430.69 177.13 o 14 0 0 1025.19 895.78 157.42 o -14 1 0 840.97 686.07 147.84 o -13 1 0 393.05 418.21 123.23 o -12 1 0 9.29 34.77 81.28 o -11 1 0 1251.09 1049.34 141.76 o -10 1 0 6343.80 6189.65 172.88 o -9 1 0 4192.50 4210.21 134.28 o -8 1 0 20.43 19.41 19.56 o -7 1 0 5069.95 4906.24 84.39 o -6 1 0 5815.07 5531.19 90.78 o -5 1 0 9094.22 9292.92 107.70 o -4 1 0 4997.60 5082.81 76.53 o -3 1 0 1113.46 1130.80 27.54 o -2 1 0 27430.13 27556.62 322.14 o 2 1 0 57249.03 58693.68 374.36 o 3 1 0 3284.85 3257.56 47.00 o 4 1 0 2811.87 2876.07 57.36 o 5 1 0 258.28 250.31 17.57 o 6 1 0 24.75 54.74 17.52 o 7 1 0 7367.37 7105.95 133.90 o 8 1 0 13859.36 14003.02 263.05 o 9 1 0 6717.90 6303.58 211.44 o 10 1 0 13.72 48.83 35.03 o 11 1 0 603.19 498.65 60.60 o 12 1 0 3553.81 3254.27 242.36 o 13 1 0 1263.58 1323.11 165.56 o 14 1 0 18.05 -55.45 89.21 o -13 2 0 1.25 -28.21 81.79 o -12 2 0 1443.58 1388.54 175.15 o -11 2 0 6137.64 6558.98 356.65 o -10 2 0 8515.00 8503.95 386.40 o -9 2 0 1092.27 1117.24 69.24 o -8 2 0 5429.68 5434.32 105.94 o -7 2 0 5232.16 5232.66 84.61 o -6 2 0 3079.28 3141.81 57.03 o -5 2 0 1687.81 1737.47 51.63 o -4 2 0 2223.84 2267.24 48.14 o -3 2 0 9834.07 9783.57 92.01 o -2 2 0 47922.00 48008.50 409.64 o -1 2 0 27424.72 27258.77 159.78 o 0 2 0 6309.67 6463.22 58.10 o 1 2 0 28766.18 29868.20 278.28 o 2 2 0 56829.86 60785.64 387.78 o 3 2 0 23307.45 23988.46 198.91 o 4 2 0 10012.36 10286.04 117.83 o 5 2 0 1120.23 1078.78 37.88 o 6 2 0 5500.20 5457.69 95.54 o 7 2 0 11974.87 11345.01 221.03 o 8 2 0 5660.56 5580.37 168.58 o 9 2 0 6.23 -5.27 37.04 o 10 2 0 1844.20 1932.57 119.24 o 11 2 0 2680.79 2567.38 124.69 o 12 2 0 1488.12 1680.92 107.95 o 13 2 0 419.44 527.87 115.45 o 14 2 0 785.66 845.87 146.47 o -13 3 0 763.94 852.82 157.48 o -12 3 0 3099.98 2965.96 264.71 o -11 3 0 3916.53 4154.39 288.31 o -10 3 0 252.53 407.46 112.90 o -9 3 0 2354.09 2490.98 209.31 o -8 3 0 3647.76 3228.93 108.54 o -7 3 0 4826.99 4558.22 68.62 o -6 3 0 1524.36 1477.26 32.70 o -5 3 0 980.78 944.17 32.96 o -4 3 0 1259.82 1045.69 76.68 o -3 3 0 39849.60 41903.93 1030.66 o -2 3 0 38230.57 37700.92 531.69 o -1 3 0 232.01 223.44 12.15 o 0 3 0 597.20 564.12 20.12 o 1 3 0 18169.39 18432.58 248.16 o 2 3 0 6387.58 6298.24 113.45 o 3 3 0 5889.26 6492.12 63.43 o 4 3 0 2426.46 2662.26 46.50 o 5 3 0 5794.95 5803.83 89.70 o 6 3 0 11067.09 11044.25 162.90 o 7 3 0 893.73 773.04 65.37 o 8 3 0 618.33 592.91 87.24 o 9 3 0 3741.60 3775.51 135.88 o 10 3 0 3468.96 3286.20 135.06 o 11 3 0 5466.49 5434.59 183.32 o 12 3 0 710.37 814.23 82.82 o 13 3 0 72.89 68.02 46.59 o 14 3 0 1600.36 1184.06 158.33 o 15 3 0 739.90 857.16 146.74 o -12 4 0 2863.06 3049.94 282.22 o -11 4 0 226.13 394.47 126.71 o -10 4 0 1744.55 1587.70 181.50 o -9 4 0 10480.05 11376.32 455.53 o -8 4 0 3970.22 4109.04 255.44 o -7 4 0 1107.86 952.43 85.56 o -6 4 0 463.51 424.28 29.60 o -5 4 0 2130.35 1914.76 61.62 o -4 4 0 9195.10 8944.44 420.66 o -3 4 0 31928.39 32548.10 761.24 o -2 4 0 7364.48 7720.61 108.26 o -1 4 0 6112.12 6252.27 91.80 o 0 4 0 18342.33 19198.08 155.08 o 1 4 0 13382.13 13224.64 128.57 o 2 4 0 3502.59 3530.01 74.48 o 3 4 0 368.82 371.19 20.61 o 4 4 0 649.21 590.47 23.52 o 5 4 0 8590.21 8799.76 109.44 o 6 4 0 10891.57 11383.95 204.98 o 7 4 0 29.05 46.33 16.87 o 8 4 0 1206.53 1243.16 73.47 o 9 4 0 6071.50 6041.83 216.58 o 10 4 0 4328.93 4260.09 153.82 o 11 4 0 1544.17 1542.29 99.51 o 12 4 0 757.72 662.78 94.24 o 13 4 0 1848.94 1810.64 118.30 o 14 4 0 1440.04 1476.78 113.00 o 15 4 0 62.70 -18.69 74.06 o -12 5 0 540.06 592.30 151.19 o -11 5 0 1004.88 1145.56 182.04 o -10 5 0 4207.92 4761.28 316.57 o -9 5 0 4177.68 4537.85 292.27 o -8 5 0 858.67 695.69 122.18 o -7 5 0 305.82 376.91 95.68 o -6 5 0 255.66 196.42 45.08 o -5 5 0 5430.59 5389.27 208.71 o -4 5 0 14248.29 12814.72 997.64 o -3 5 0 1064.04 1017.07 39.16 o -2 5 0 12800.22 14085.33 285.16 o -1 5 0 29125.53 30604.97 499.65 o 0 5 0 7529.25 7527.24 94.02 o 1 5 0 9333.08 10051.38 114.84 o 2 5 0 8771.35 9543.31 110.04 o 3 5 0 884.68 992.51 65.89 o 4 5 0 3130.79 3205.31 110.33 o 5 5 0 204.30 239.66 15.91 o 6 5 0 377.43 514.40 26.27 o 7 5 0 3872.67 3832.62 143.37 o 8 5 0 2184.02 2300.30 108.04 o 9 5 0 3129.97 3097.49 115.30 o 10 5 0 1429.35 1274.09 70.18 o 11 5 0 12.03 -33.99 33.99 o 12 5 0 2942.72 2887.37 129.34 o 13 5 0 1450.57 1490.64 89.30 o 14 5 0 61.06 20.54 65.78 o 15 5 0 132.54 262.45 103.83 o -11 6 0 1871.03 1833.48 226.10 o -10 6 0 2590.28 2841.13 258.41 o -9 6 0 683.44 662.75 130.48 o -8 6 0 122.77 104.30 73.94 o -7 6 0 569.06 501.43 107.58 o -6 6 0 2602.60 2760.44 202.91 o -5 6 0 4019.71 3880.03 271.93 o -4 6 0 860.24 781.30 47.71 o -3 6 0 889.12 875.28 32.51 o -2 6 0 10476.50 10053.44 305.10 o -1 6 0 10025.13 10742.35 145.05 o 0 6 0 2267.93 2185.10 50.49 o 1 6 0 507.14 464.69 24.97 o 2 6 0 827.12 838.17 33.30 o 3 6 0 4952.10 4822.17 189.32 o 4 6 0 10611.43 11300.72 317.54 o 5 6 0 31.02 42.23 41.84 o 6 6 0 1499.41 1467.95 66.46 o 7 6 0 2686.70 2836.74 84.46 o 8 6 0 3072.59 3008.48 107.89 o 9 6 0 2773.36 2733.59 93.69 o 10 6 0 241.78 239.20 39.00 o 11 6 0 2033.93 2171.50 118.58 o 12 6 0 4818.22 4685.00 223.32 o 13 6 0 609.62 520.21 91.21 o 14 6 0 464.04 309.58 89.95 o 15 6 0 358.23 262.01 65.18 o -10 7 0 645.87 714.85 153.74 o -9 7 0 20.06 13.98 89.40 o -8 7 0 469.57 676.42 130.09 o -7 7 0 1259.58 1210.36 154.50 o -6 7 0 3044.55 3302.27 232.67 o -5 7 0 833.90 827.45 76.92 o -4 7 0 410.58 497.39 92.35 o -3 7 0 2351.11 2231.64 56.25 o -2 7 0 5984.57 6467.82 137.69 o -1 7 0 1895.00 1799.00 55.78 o 0 7 0 912.30 953.38 36.03 o 2 7 0 7490.96 7897.28 121.36 o 3 7 0 4549.07 4616.93 178.66 o 4 7 0 400.51 489.97 70.83 o 5 7 0 1473.15 1556.60 124.60 o 6 7 0 704.71 786.20 68.15 o 7 7 0 1262.03 1325.78 49.28 o 8 7 0 2035.72 2150.31 105.39 o 9 7 0 251.86 245.38 33.66 o 10 7 0 777.58 816.48 61.21 o 11 7 0 5191.80 5158.37 144.32 o 12 7 0 1851.81 1808.40 122.11 o 13 7 0 60.48 98.85 53.83 o 14 7 0 566.27 304.82 63.51 o 15 7 0 346.31 415.45 78.13 o -10 8 0 8.17 -44.88 113.54 o -9 8 0 55.47 -103.34 103.34 o -8 8 0 1343.44 1301.39 183.18 o -7 8 0 1775.34 1875.73 195.71 o -6 8 0 437.70 578.35 114.54 o -5 8 0 69.32 72.29 64.11 o -4 8 0 2387.47 2157.34 175.95 o -3 8 0 1939.72 2051.26 73.63 o -2 8 0 1092.18 987.75 52.53 o -1 8 0 845.14 780.65 39.47 o 0 8 0 883.83 959.46 53.38 o 1 8 0 4452.73 4600.22 107.15 o 2 8 0 6427.96 6461.54 229.82 o 3 8 0 148.80 145.57 22.10 o 4 8 0 6055.31 5518.28 236.01 o 5 8 0 2358.90 2465.07 160.07 o 6 8 0 411.06 421.58 81.11 o 7 8 0 380.37 399.80 56.89 o 8 8 0 443.71 381.67 55.15 o 9 8 0 2864.14 2976.87 87.88 o 10 8 0 6784.45 7112.70 227.60 o 11 8 0 3797.54 4123.80 179.54 o 12 8 0 400.30 338.09 62.12 o 13 8 0 592.77 586.79 149.96 o 14 8 0 674.36 660.13 88.26 o 15 8 0 379.53 259.09 69.27 o -9 9 0 518.38 735.76 160.46 o -8 9 0 1546.82 1635.03 197.25 o -7 9 0 891.22 1107.89 163.71 o -6 9 0 18.92 13.52 75.97 o -5 9 0 260.31 400.51 100.95 o -4 9 0 1159.49 1565.35 160.39 o -3 9 0 1089.47 1041.33 57.61 o -2 9 0 1961.28 1901.20 77.59 o -1 9 0 55.26 66.05 34.82 o 0 9 0 1419.34 1431.88 67.16 o 1 9 0 5018.46 5195.79 126.68 o 2 9 0 1080.10 1008.76 48.98 o 3 9 0 1136.40 1039.58 42.85 o 4 9 0 1680.39 1599.11 93.58 o 5 9 0 167.32 54.31 58.34 o 6 9 0 89.42 -14.15 62.04 o 7 9 0 555.25 542.19 29.55 o 8 9 0 44.50 59.21 69.00 o 9 9 0 4656.25 5192.09 469.92 o 10 9 0 3995.18 4435.26 502.84 o 11 9 0 52.80 73.73 106.36 o 12 9 0 493.05 413.21 95.51 o 13 9 0 661.79 709.39 94.10 o 14 9 0 322.66 243.63 82.79 o -8 10 0 348.94 152.98 108.22 o -7 10 0 25.06 39.51 80.97 o -6 10 0 981.94 1034.29 154.17 o -5 10 0 1043.20 1352.47 164.63 o -4 10 0 341.32 455.29 102.83 o -3 10 0 339.06 324.43 123.06 o -2 10 0 72.86 125.31 47.28 o -1 10 0 3511.39 3635.19 113.57 o 0 10 0 10005.79 10424.85 277.70 o 1 10 0 2391.66 2432.20 90.49 o 2 10 0 57.85 48.98 10.67 o 3 10 0 924.34 1002.72 45.89 o 4 10 0 489.67 449.63 27.80 o 5 10 0 109.57 71.30 60.48 o 6 10 0 66.01 -2.79 62.57 o 7 10 0 257.19 30.52 69.74 o 8 10 0 2719.16 2761.19 207.21 o 9 10 0 7095.44 7902.03 361.04 o 10 10 0 1799.13 2143.11 132.77 o 11 10 0 130.32 3.37 65.68 o 12 10 0 1014.89 1260.06 115.51 o 13 10 0 1197.18 1162.33 112.15 o 14 10 0 829.70 907.40 274.17 o -7 11 0 193.56 164.38 100.49 o -6 11 0 520.07 583.10 136.59 o -5 11 0 567.07 753.14 131.14 o -4 11 0 368.83 400.53 93.40 o -3 11 0 107.65 64.09 50.51 o -2 11 0 690.89 801.15 118.11 o -1 11 0 4289.92 4095.59 127.03 o 0 11 0 3173.67 3283.47 113.51 o 1 11 0 285.06 308.75 41.05 o 2 11 0 3437.24 3511.68 243.53 o 3 11 0 511.24 541.83 37.63 o 4 11 0 163.34 106.41 52.99 o 5 11 0 273.84 213.51 42.94 o 6 11 0 37.21 -30.99 77.43 o 7 11 0 1885.14 1810.32 174.16 o 8 11 0 5691.06 5532.15 302.77 o 9 11 0 2002.39 2077.22 196.76 o 10 11 0 323.78 276.70 99.06 o 11 11 0 1498.27 1436.31 179.20 o 12 11 0 975.78 551.42 126.75 o 13 11 0 408.30 376.62 163.98 o -5 12 0 90.23 -40.42 93.92 o -4 12 0 4.54 72.10 73.43 o -3 12 0 470.15 525.06 86.36 o -2 12 0 1350.65 1475.81 332.94 o -1 12 0 2033.01 2391.79 138.22 o 0 12 0 1.76 7.98 38.74 o 1 12 0 2743.01 2778.56 106.92 o 2 12 0 2865.27 2975.78 148.84 o 3 12 0 1070.58 791.39 109.54 o 4 12 0 8.37 -67.77 69.96 o 5 12 0 69.97 76.62 69.02 o 6 12 0 1316.71 1262.89 145.46 o 7 12 0 4824.60 5089.35 290.70 o 8 12 0 1333.66 1217.30 157.16 o 9 12 0 4.98 17.01 76.61 o 10 12 0 2373.30 2150.62 209.68 o 11 12 0 1387.58 1252.48 173.64 o 12 12 0 908.04 1083.73 164.01 o 13 12 0 132.66 97.75 87.89 o -4 13 0 47.87 46.79 76.60 o -3 13 0 1301.67 1468.19 171.82 o -2 13 0 1565.32 1640.72 129.29 o -1 13 0 202.05 245.64 61.09 o 0 13 0 1603.08 1609.50 192.39 o 1 13 0 1162.15 1153.20 101.11 o 2 13 0 435.92 604.32 115.56 o 3 13 0 66.43 -67.26 67.26 o 4 13 0 14.92 123.72 71.54 o 5 13 0 244.84 190.96 85.60 o 6 13 0 1780.25 2050.11 189.71 o 7 13 0 1619.41 1985.91 194.31 o 8 13 0 151.88 33.15 89.05 o 9 13 0 1456.17 1734.91 194.35 o 10 13 0 3012.60 2607.97 239.10 o 11 13 0 1286.40 1562.59 198.98 o 12 13 0 362.88 201.77 99.65 o -2 14 0 127.11 122.23 112.22 o -1 14 0 738.94 1002.86 173.77 o 0 14 0 1640.00 1724.82 205.94 o 1 14 0 362.58 387.85 110.62 o 2 14 0 38.88 100.75 54.93 o 3 14 0 22.39 26.48 52.07 o 4 14 0 1171.06 1116.51 141.33 o 5 14 0 1487.55 1513.13 169.10 o 6 14 0 1911.34 2117.44 200.32 o 7 14 0 10.14 -28.73 79.54 o 8 14 0 1189.01 1030.67 157.96 o 9 14 0 2171.71 2138.87 221.26 o 10 14 0 1221.75 1075.34 166.81 o 11 14 0 342.33 231.41 116.18 o 0 15 0 828.32 943.96 175.89 o 1 15 0 47.06 77.21 92.20 o 2 15 0 22.66 -126.75 126.75 o 3 15 0 28.11 -45.26 59.76 o 4 15 0 685.34 991.94 139.53 o 5 15 0 640.69 818.10 142.72 o 6 15 0 61.98 85.47 85.03 o 7 15 0 696.60 997.89 154.19 o 8 15 0 2381.83 2509.34 237.00 o 9 15 0 1108.95 1363.36 187.17 o 4 16 0 514.34 581.43 95.78 o 5 16 0 0.82 19.61 74.04 o 6 16 0 799.05 738.27 140.68 o -6 -16 1 1630.90 1538.96 186.02 o -5 -16 1 137.19 362.12 114.39 o -4 -16 1 129.38 43.26 58.07 o -9 -15 1 214.02 205.89 97.89 o -8 -15 1 767.80 855.73 148.63 o -7 -15 1 1500.78 1633.53 194.60 o -6 -15 1 836.50 712.39 136.14 o -5 -15 1 158.12 271.13 104.25 o -4 -15 1 1075.28 1117.92 145.95 o -3 -15 1 178.39 268.18 73.00 o -2 -15 1 24.32 7.60 101.15 o -1 -15 1 42.34 -94.37 94.37 o 0 -15 1 32.43 -85.09 98.87 o -11 -14 1 19.65 -84.88 84.88 o -10 -14 1 81.46 1.11 105.19 o -9 -14 1 1406.35 1472.08 189.49 o -8 -14 1 1589.91 1680.16 189.97 o -7 -14 1 1169.60 1166.89 159.82 o -6 -14 1 40.46 112.85 75.22 o -5 -14 1 767.74 565.25 111.13 o -4 -14 1 1354.22 1247.12 152.12 o -3 -14 1 193.39 75.07 52.37 o -2 -14 1 33.45 6.99 48.27 o -1 -14 1 23.01 -18.04 62.31 o 0 -14 1 381.91 352.96 111.01 o 1 -14 1 732.15 875.10 161.51 o 2 -14 1 103.56 83.64 87.80 o -12 -13 1 36.54 -118.41 118.41 o -11 -13 1 10.72 -66.60 96.44 o -10 -13 1 283.94 516.45 125.94 o -9 -13 1 1798.40 1877.84 199.90 o -8 -13 1 756.40 536.58 120.18 o -7 -13 1 31.08 13.92 80.98 o -6 -13 1 1930.30 2279.28 198.50 o -5 -13 1 1728.21 1602.72 166.45 o -4 -13 1 98.70 181.32 85.69 o -3 -13 1 20.89 13.10 59.38 o -2 -13 1 250.30 243.56 55.72 o -1 -13 1 98.06 80.21 106.17 o 0 -13 1 781.39 704.10 80.32 o 1 -13 1 351.42 442.72 72.76 o 2 -13 1 124.12 104.94 55.19 o 3 -13 1 725.60 566.00 87.38 o 4 -13 1 688.48 670.00 128.03 o -13 -12 1 412.27 154.59 103.22 o -12 -12 1 5.75 -44.90 96.03 o -11 -12 1 216.02 110.24 92.40 o -10 -12 1 1109.53 1076.21 156.38 o -9 -12 1 1005.68 870.53 142.07 o -8 -12 1 4.77 -69.03 73.92 o -7 -12 1 770.27 681.50 120.52 o -6 -12 1 1568.63 1738.78 168.56 o -5 -12 1 564.70 759.52 111.49 o -4 -12 1 10.59 -49.91 66.49 o -3 -12 1 97.25 -61.91 73.08 o -2 -12 1 151.76 138.60 51.60 o -1 -12 1 1148.56 1231.22 73.15 o 0 -12 1 312.49 352.51 45.57 o 1 -12 1 29.43 21.06 37.63 o 2 -12 1 1284.77 1303.92 172.39 o 3 -12 1 936.41 1022.11 105.33 o 4 -12 1 545.41 547.52 113.73 o 5 -12 1 12.78 -69.30 97.73 o 6 -12 1 26.90 -53.12 82.60 o -13 -11 1 3.73 2.91 64.05 o -12 -11 1 91.67 48.34 68.01 o -11 -11 1 912.36 956.14 143.63 o -10 -11 1 1031.97 817.93 132.58 o -9 -11 1 323.25 288.74 91.81 o -8 -11 1 2017.64 2203.55 193.12 o -7 -11 1 1603.72 1733.91 172.26 o -6 -11 1 1908.78 1995.29 175.40 o -5 -11 1 183.98 154.22 27.92 o -4 -11 1 208.57 142.32 41.53 o -3 -11 1 255.26 389.40 70.92 o -2 -11 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