[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o1551-o1552
[ doi:10.1107/S1600536813025336 ]

(3aR,6S,7aR)-7a-Chloro-2-[(4-nitrophenyl)sulfonyl]-1,2,3,6,7,7a-hexahydro-3a,6-epoxyisoindole

E. Temel, A. Demircan, M. K. Kandemir, M. Çolak and O. Büyükgüngör


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B RINTA01_ALERT_3_B The value of Rint is greater than 0.18 Rint given 0.242
Alert level C PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 6.871 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 2 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 2
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size .... 0.68 mm PLAT343_ALERT_2_G Check sp3 Angle Range in Main Residue for .. C8 PLAT793_ALERT_4_G The Model has Chirality at C8 (Verify) .... R PLAT793_ALERT_4_G The Model has Chirality at C11 (Verify) .... S PLAT793_ALERT_4_G The Model has Chirality at C13 (Verify) .... R
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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