[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o1589-o1590
[ doi:10.1107/S1600536813025543 ]

N-(1-Allyl-1H-indazol-5-yl)-4-methoxybenzenesulfonamide hemihydrate

H. Chicha, E. M. Rakib, D. Geffken, M. Saadi and L. El Ammari

Key indicators

checkCIF/PLATON results

No syntax errors found

Alert level C PLAT230_ALERT_2_C Hirshfeld Test Diff for C11 -- C16 .. 5.6 su PLAT420_ALERT_2_C D-H Without Acceptor *N1' - *H1' ... ? Check PLAT480_ALERT_4_C Long H...A H-Bond Reported H7 .. O2 .. 2.63 Ang. PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -0.155 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 4 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT007_ALERT_5_G Note: Number of Unrefined Donor-H Atoms ........ 4 PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 17 % PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 100 % PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... ! Info PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 2
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 7 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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