[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m534-m535
[ doi:10.1107/S1600536813023933 ]

[[mu]-3,3'-Bis(trihydroboryl)[3]ferrocenophane]bis(chloridozirconocene)

A. Reichert, H.-W. Lerner, M. Wagner and M. Bolte


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT201_ALERT_2_B Isotropic non-H Atoms in Main Residue(s) ....... 1 PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 11
Alert level C PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C6 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C8 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C21 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C35 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C37 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C40 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Zr1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Zr2 PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0104 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 15.394 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.795 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Zr1 -- Cl1 .. 22.8 su PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C7 PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C7' PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 3 % PLAT303_ALERT_2_G Full Occupancy H-Atom H1A with # Connections 2.00 PLAT303_ALERT_2_G Full Occupancy H-Atom H1B with # Connections 2.00 PLAT303_ALERT_2_G Full Occupancy H-Atom H2A with # Connections 2.00 PLAT303_ALERT_2_G Full Occupancy H-Atom H2B with # Connections 2.00 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 32
0 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 12 ALERT level C = Check. Ensure it is not caused by an omission or oversight 10 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 16 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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