# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared), status flag # data_I _shelx_title ' 10039 in Cc' _shelx_refln_list_code 4 _shelx_F_calc_maximum 384.09 _exptl_crystal_F_000 1708.00 _reflns_d_resolution_high 0.7479 loop_ _space_group_symop_operation_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' _cell_length_a 22.2870 _cell_length_b 12.6760 _cell_length_c 13.3390 _cell_angle_alpha 90.000 _cell_angle_beta 98.510 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -3 1 -17 25.99 -151.37 151.37 o -1 1 -17 481.72 388.71 180.41 o 1 1 -17 198.52 295.64 181.83 o 3 1 -17 37.66 149.12 268.54 o 5 1 -17 40.77 70.60 171.52 o 7 1 -17 21.47 51.01 208.13 o 9 1 -17 902.00 636.88 232.38 o 11 1 -17 56.33 -100.72 195.35 o -2 2 -17 35.43 1935.83 1707.61 o 0 2 -17 99.73 149.24 171.91 o 2 2 -17 219.59 115.41 448.21 o 4 2 -17 1142.77 674.69 429.02 o 6 2 -17 611.24 621.89 341.42 o 8 2 -17 385.49 510.53 219.66 o 10 2 -17 208.64 273.21 357.07 o -1 3 -17 151.95 849.77 241.81 o 1 3 -17 706.71 1066.24 249.53 o 3 3 -17 69.36 -102.07 165.02 o 5 3 -17 93.93 41.33 175.30 o 7 3 -17 188.50 479.68 209.58 o 9 3 -17 210.93 172.02 210.94 o 11 3 -17 40.60 197.69 349.09 o 0 4 -17 156.82 420.28 509.96 o 2 4 -17 218.12 5.31 235.90 o 4 4 -17 1.49 -63.75 307.22 o 6 4 -17 444.54 152.80 189.30 o 8 4 -17 682.31 1012.22 378.12 o -8 0 -16 93.05 -146.30 249.66 o -6 0 -16 39.67 -20.76 237.67 o -4 0 -16 216.82 58.67 234.19 o -2 0 -16 1901.30 1316.37 335.76 o 0 0 -16 974.66 769.92 282.70 o 2 0 -16 67.88 102.05 209.14 o 4 0 -16 503.04 565.45 257.12 o 6 0 -16 63.36 -58.94 222.68 o 8 0 -16 331.10 175.23 247.02 o 10 0 -16 316.40 353.32 275.30 o 12 0 -16 3767.17 3217.45 533.04 o 14 0 -16 301.97 47.65 289.62 o 16 0 -16 189.22 369.43 245.01 o -7 1 -16 33.80 449.08 246.29 o -5 1 -16 691.61 1007.42 232.20 o -3 1 -16 153.73 156.19 181.78 o -1 1 -16 431.60 -71.92 146.81 o 1 1 -16 1405.73 1404.08 227.84 o 3 1 -16 1050.86 1102.13 429.38 o 5 1 -16 88.37 82.04 144.62 o 7 1 -16 205.89 379.28 168.89 o 9 1 -16 556.57 724.22 225.99 o 11 1 -16 627.91 788.67 229.50 o 13 1 -16 402.40 186.75 292.61 o 15 1 -16 137.08 46.99 169.29 o -8 2 -16 113.01 266.55 246.24 o -6 2 -16 107.40 78.59 192.63 o -4 2 -16 237.35 302.81 190.18 o -2 2 -16 378.45 228.48 295.35 o 0 2 -16 1500.72 1377.19 244.81 o 2 2 -16 1879.51 1627.57 305.87 o 4 2 -16 953.01 857.38 357.08 o 6 2 -16 2004.29 1732.30 269.37 o 8 2 -16 222.56 113.03 171.76 o 10 2 -16 200.70 -80.66 166.91 o 12 2 -16 484.97 125.98 161.57 o 14 2 -16 227.25 209.08 170.97 o 16 2 -16 403.96 390.27 208.99 o -7 3 -16 190.69 151.95 202.36 o -5 3 -16 466.71 602.34 210.53 o -3 3 -16 427.99 535.28 196.12 o -1 3 -16 251.64 111.51 172.72 o 1 3 -16 2120.29 2158.05 302.88 o 3 3 -16 772.08 831.53 207.47 o 5 3 -16 314.92 272.84 173.67 o 7 3 -16 803.89 522.88 192.90 o 9 3 -16 1486.17 1551.60 256.19 o 11 3 -16 956.52 1008.31 257.82 o 13 3 -16 119.17 -192.62 192.62 o 15 3 -16 307.74 396.16 195.04 o -6 4 -16 790.54 870.82 256.52 o -4 4 -16 141.88 68.60 197.72 o -2 4 -16 80.55 193.51 263.16 o 0 4 -16 519.00 176.05 190.24 o 2 4 -16 626.58 337.51 191.67 o 4 4 -16 53.75 41.12 153.46 o 6 4 -16 66.86 328.67 176.84 o 8 4 -16 747.43 901.60 210.65 o 10 4 -16 2205.19 2695.98 366.14 o 12 4 -16 474.74 356.26 342.29 o 14 4 -16 558.08 728.44 275.69 o -5 5 -16 286.78 501.30 212.04 o -3 5 -16 197.60 366.51 203.87 o -1 5 -16 339.91 369.29 212.47 o 1 5 -16 300.59 -58.48 178.72 o 3 5 -16 355.34 581.57 220.10 o 5 5 -16 235.83 325.97 187.49 o 7 5 -16 13.26 119.49 267.38 o 9 5 -16 264.84 308.83 213.35 o 11 5 -16 799.21 659.51 245.77 o 13 5 -16 655.90 1232.88 542.88 o -2 6 -16 59.87 72.16 260.63 o 0 6 -16 1247.17 1458.62 275.59 o 2 6 -16 403.84 -132.93 418.25 o 4 6 -16 825.42 490.74 223.91 o 6 6 -16 3.03 -113.89 170.32 o 8 6 -16 3.00 -20.17 217.85 o 10 6 -16 554.74 515.25 437.04 o 1 7 -16 49.16 -14.13 243.53 o 3 7 -16 1139.62 1613.04 451.76 o 5 7 -16 243.70 303.41 232.88 o 7 7 -16 55.00 102.21 216.96 o -11 1 -15 292.73 329.30 216.94 o -9 1 -15 96.95 125.05 171.83 o -7 1 -15 9.86 -35.33 159.58 o -5 1 -15 73.32 347.78 172.26 o -3 1 -15 671.39 354.94 162.45 o -1 1 -15 141.53 151.61 142.86 o 1 1 -15 303.74 103.69 130.63 o 3 1 -15 293.00 162.43 135.27 o 5 1 -15 55.44 -13.67 125.78 o 7 1 -15 44.37 -105.87 140.62 o 9 1 -15 1299.91 1241.76 367.66 o 11 1 -15 432.97 232.25 179.12 o 13 1 -15 1229.33 1146.41 202.06 o 15 1 -15 307.59 400.80 149.54 o 17 1 -15 47.77 56.23 190.56 o 19 1 -15 296.65 313.73 235.71 o -10 2 -15 187.15 -29.90 374.26 o -8 2 -15 141.64 167.83 188.09 o -6 2 -15 4.97 134.45 151.83 o -4 2 -15 60.42 225.28 182.17 o -2 2 -15 1.78 -112.28 230.45 o 0 2 -15 605.49 515.36 172.72 o 2 2 -15 180.53 423.95 152.21 o 4 2 -15 57.88 -54.33 154.69 o 6 2 -15 420.99 373.45 159.32 o 8 2 -15 240.56 280.48 192.33 o 10 2 -15 443.43 340.03 226.77 o 12 2 -15 314.75 256.94 152.41 o 14 2 -15 1191.91 899.24 186.91 o 16 2 -15 133.99 46.27 166.44 o 18 2 -15 55.48 -168.80 168.80 o -11 3 -15 33.18 405.52 314.59 o -9 3 -15 98.55 272.71 199.46 o -7 3 -15 102.73 -37.98 162.49 o -5 3 -15 105.36 180.12 251.80 o -3 3 -15 335.91 340.58 217.80 o -1 3 -15 10.88 210.49 165.33 o 1 3 -15 135.90 234.91 221.84 o 3 3 -15 511.97 369.90 163.21 o 5 3 -15 107.07 7.08 130.31 o 7 3 -15 0.23 162.79 306.42 o 9 3 -15 8.98 19.56 146.95 o 11 3 -15 36.72 295.74 149.65 o 13 3 -15 473.87 610.04 223.02 o 15 3 -15 529.50 498.74 175.99 o 17 3 -15 150.34 190.07 171.25 o -10 4 -15 573.44 159.86 216.60 o -8 4 -15 514.58 545.80 248.40 o -6 4 -15 230.85 373.86 401.04 o -4 4 -15 388.39 449.31 222.56 o -2 4 -15 64.01 171.62 166.42 o 0 4 -15 353.99 556.96 187.24 o 2 4 -15 595.36 257.75 247.81 o 4 4 -15 808.58 765.83 186.65 o 6 4 -15 127.79 86.61 141.54 o 8 4 -15 448.10 737.58 229.90 o 10 4 -15 41.85 76.09 175.79 o 12 4 -15 602.79 614.02 228.85 o 14 4 -15 11.42 208.60 202.19 o 16 4 -15 50.25 124.54 186.95 o -9 5 -15 1023.79 717.03 374.54 o -7 5 -15 7.08 154.15 192.19 o -5 5 -15 214.15 -2.91 261.06 o -3 5 -15 256.55 343.37 327.37 o -1 5 -15 42.59 120.18 165.97 o 1 5 -15 641.99 330.33 182.95 o 3 5 -15 660.12 873.96 230.14 o 5 5 -15 475.13 426.52 176.83 o 7 5 -15 360.42 586.65 192.79 o 9 5 -15 128.52 172.76 185.93 o 11 5 -15 836.60 750.75 478.39 o 13 5 -15 332.47 309.16 223.91 o 15 5 -15 58.30 2.97 165.07 o -8 6 -15 667.81 827.95 275.95 o -6 6 -15 40.61 120.75 194.02 o -4 6 -15 65.62 151.67 195.20 o -2 6 -15 979.42 1306.97 264.03 o 0 6 -15 252.21 120.29 180.04 o 2 6 -15 1049.26 927.26 394.04 o 4 6 -15 232.39 214.56 196.60 o 6 6 -15 402.10 -50.06 173.71 o 8 6 -15 264.94 94.09 181.23 o 10 6 -15 283.74 405.01 211.42 o 12 6 -15 279.64 227.52 219.87 o 14 6 -15 257.19 789.21 379.19 o -5 7 -15 1102.04 1637.33 315.49 o -3 7 -15 138.85 436.78 228.35 o -1 7 -15 243.21 -84.01 259.13 o 1 7 -15 1082.87 1117.06 296.30 o 3 7 -15 316.63 228.32 264.46 o 5 7 -15 253.99 63.72 196.30 o 7 7 -15 114.32 -75.44 190.45 o 9 7 -15 110.39 69.29 212.21 o 11 7 -15 578.12 488.89 236.01 o 13 7 -15 55.40 151.95 231.85 o -2 8 -15 178.55 -213.09 224.88 o 0 8 -15 340.14 98.36 368.43 o 2 8 -15 801.58 715.67 246.02 o 4 8 -15 385.82 422.55 428.98 o 6 8 -15 79.17 -201.81 347.06 o 8 8 -15 657.87 586.88 269.85 o 10 8 -15 50.62 164.26 234.02 o 3 9 -15 74.51 -308.22 308.22 o 5 9 -15 78.16 -61.94 238.93 o -14 0 -14 510.39 577.54 247.78 o -12 0 -14 321.11 259.92 284.48 o -10 0 -14 924.56 1089.47 321.85 o -8 0 -14 186.43 144.83 195.97 o -6 0 -14 627.25 664.33 250.36 o -4 0 -14 385.45 494.18 222.55 o -2 0 -14 216.45 378.90 234.21 o 0 0 -14 2382.69 2909.05 380.95 o 2 0 -14 2365.49 1891.23 348.35 o 4 0 -14 55.07 192.84 181.74 o 6 0 -14 131.46 474.77 213.21 o 8 0 -14 511.25 -18.95 175.07 o 10 0 -14 2562.99 2171.02 386.65 o 12 0 -14 2495.85 2232.86 412.03 o 14 0 -14 2320.77 2295.94 310.04 o 16 0 -14 478.51 342.48 202.34 o 18 0 -14 961.24 307.92 305.06 o 20 0 -14 1242.32 848.25 371.94 o -13 1 -14 376.03 215.41 171.85 o -11 1 -14 601.20 462.85 196.99 o -9 1 -14 157.83 -72.97 144.80 o -7 1 -14 248.03 270.96 160.47 o -5 1 -14 575.08 558.04 180.21 o -3 1 -14 137.77 -44.03 119.65 o -1 1 -14 288.22 89.49 128.05 o 1 1 -14 1292.19 1245.54 245.00 o 3 1 -14 417.38 422.16 144.30 o 5 1 -14 426.37 330.32 129.78 o 7 1 -14 163.53 17.66 121.41 o 9 1 -14 255.19 180.47 135.23 o 11 1 -14 2415.20 2071.92 268.43 o 13 1 -14 1183.28 812.61 180.82 o 15 1 -14 427.77 378.28 132.56 o 17 1 -14 370.52 659.68 189.10 o 19 1 -14 718.18 634.16 190.36 o 21 1 -14 430.90 211.38 232.04 o -14 2 -14 296.48 530.33 210.93 o -12 2 -14 537.49 573.19 179.83 o -10 2 -14 901.70 1288.31 259.42 o -8 2 -14 1020.92 1364.33 581.65 o -6 2 -14 335.51 91.77 147.11 o -4 2 -14 1637.26 1409.25 370.73 o -2 2 -14 605.74 855.16 293.21 o 0 2 -14 143.05 90.10 123.92 o 2 2 -14 2106.79 1509.05 288.61 o 4 2 -14 225.22 244.07 191.25 o 6 2 -14 623.34 313.05 137.38 o 8 2 -14 934.90 752.45 179.21 o 10 2 -14 71.89 81.70 140.08 o 12 2 -14 790.98 666.11 163.30 o 14 2 -14 727.20 672.01 163.97 o 16 2 -14 174.93 -29.69 140.54 o 18 2 -14 457.65 594.82 192.74 o 20 2 -14 252.94 -26.32 180.25 o -13 3 -14 359.41 320.67 185.85 o -11 3 -14 498.37 422.35 301.71 o -9 3 -14 716.18 1236.06 227.00 o -7 3 -14 679.69 1024.19 211.28 o -5 3 -14 2070.34 1799.53 371.43 o -3 3 -14 2280.07 1968.62 336.36 o -1 3 -14 1128.17 815.28 350.71 o 1 3 -14 882.14 551.66 163.89 o 3 3 -14 1350.10 1018.42 221.60 o 5 3 -14 1616.15 1440.50 264.93 o 7 3 -14 1974.33 2007.00 337.09 o 9 3 -14 7288.77 7299.63 432.78 o 11 3 -14 3154.86 3308.24 284.86 o 13 3 -14 2187.56 2103.20 640.42 o 15 3 -14 145.59 -21.90 134.97 o 17 3 -14 1869.50 1899.68 402.61 o 19 3 -14 296.67 129.24 186.85 o -12 4 -14 142.78 438.82 426.50 o -10 4 -14 85.67 143.57 158.69 o -8 4 -14 146.55 -144.32 156.23 o -6 4 -14 150.20 165.44 157.39 o -4 4 -14 1763.77 1582.05 255.36 o -2 4 -14 272.75 435.84 176.74 o 0 4 -14 119.09 -19.06 141.56 o 2 4 -14 209.95 274.00 157.50 o 4 4 -14 2913.05 3195.99 289.70 o 6 4 -14 369.88 217.24 146.67 o 8 4 -14 3755.34 3318.36 311.09 o 10 4 -14 1709.84 1804.51 208.45 o 12 4 -14 2818.53 2683.61 478.62 o 14 4 -14 3281.98 2843.85 634.28 o 16 4 -14 104.65 102.09 163.04 o 18 4 -14 148.07 140.42 173.64 o 20 4 -14 1345.90 1240.93 253.98 o -11 5 -14 110.61 310.29 205.55 o -9 5 -14 28.91 56.33 375.66 o -7 5 -14 24.96 -24.63 166.00 o -5 5 -14 172.95 286.23 178.43 o -3 5 -14 107.97 361.52 170.85 o -1 5 -14 71.62 278.35 174.34 o 1 5 -14 201.79 98.08 149.94 o 3 5 -14 3619.67 3936.61 334.07 o 5 5 -14 982.06 563.80 252.77 o 7 5 -14 113.94 1.08 132.64 o 9 5 -14 99.42 423.25 185.66 o 11 5 -14 1240.78 1076.98 240.37 o 13 5 -14 589.84 620.47 230.30 o 15 5 -14 964.00 785.46 196.91 o 17 5 -14 121.40 96.94 169.56 o 19 5 -14 684.87 765.64 393.92 o -10 6 -14 142.37 101.45 307.45 o -8 6 -14 1169.94 1117.12 290.44 o -6 6 -14 1109.52 985.65 285.52 o -4 6 -14 156.62 220.45 163.64 o -2 6 -14 85.65 185.38 172.27 o 0 6 -14 79.76 208.12 167.21 o 2 6 -14 5769.96 5929.70 422.09 o 4 6 -14 1115.61 842.45 217.15 o 6 6 -14 1233.77 1096.51 174.53 o 8 6 -14 127.53 28.81 193.23 o 10 6 -14 830.48 878.61 402.71 o 12 6 -14 1092.71 817.96 258.32 o 14 6 -14 562.70 144.55 201.06 o 16 6 -14 172.43 387.00 234.65 o 18 6 -14 845.71 723.00 289.99 o -9 7 -14 256.64 647.73 233.42 o -7 7 -14 2277.37 2320.79 498.46 o -5 7 -14 540.92 655.13 234.24 o -3 7 -14 304.43 138.17 303.43 o -1 7 -14 65.75 88.39 183.97 o 1 7 -14 25.20 -5.97 170.20 o 3 7 -14 56.04 2.22 153.01 o 5 7 -14 1475.33 1455.46 267.93 o 7 7 -14 59.84 131.70 179.08 o 9 7 -14 291.51 371.44 212.82 o 11 7 -14 988.72 941.67 261.38 o 13 7 -14 343.31 201.69 210.03 o 15 7 -14 64.45 209.56 235.16 o -8 8 -14 23.85 187.28 218.60 o -6 8 -14 470.87 562.43 368.33 o -4 8 -14 91.61 282.16 204.30 o -2 8 -14 268.67 55.54 358.88 o 0 8 -14 135.39 -11.97 241.39 o 2 8 -14 881.39 1009.45 252.98 o 4 8 -14 317.36 380.91 208.06 o 6 8 -14 110.15 152.00 199.70 o 8 8 -14 376.02 265.76 218.74 o 10 8 -14 1356.19 1545.70 306.44 o 12 8 -14 410.09 574.39 238.94 o 14 8 -14 524.70 914.93 866.57 o -5 9 -14 225.48 118.42 363.65 o -3 9 -14 82.41 354.92 353.89 o -1 9 -14 1354.40 1675.90 308.13 o 1 9 -14 52.89 247.69 279.57 o 3 9 -14 449.83 471.34 287.83 o 5 9 -14 753.58 766.42 265.54 o 7 9 -14 591.26 171.92 263.20 o 9 9 -14 1849.83 1719.44 329.95 o 11 9 -14 1631.34 1427.65 303.11 o 0 10 -14 192.70 360.40 328.90 o 2 10 -14 176.36 201.19 334.32 o 4 10 -14 666.97 729.45 383.99 o 6 10 -14 1900.14 2239.64 515.31 o 8 10 -14 522.85 591.39 277.60 o -15 1 -13 23.68 32.53 137.05 o -13 1 -13 345.80 394.55 139.91 o -11 1 -13 1968.98 1837.95 204.14 o -9 1 -13 844.28 623.46 144.51 o -7 1 -13 534.01 367.07 270.47 o -5 1 -13 20.07 42.61 116.55 o -3 1 -13 121.14 265.90 130.22 o -1 1 -13 68.15 -38.42 100.74 o 1 1 -13 532.55 525.50 147.81 o 3 1 -13 172.42 225.64 116.96 o 5 1 -13 498.46 258.74 204.53 o 7 1 -13 1102.18 1294.28 458.48 o 9 1 -13 377.75 497.07 148.02 o 11 1 -13 100.85 146.76 143.33 o 13 1 -13 617.78 595.41 152.76 o 15 1 -13 250.62 426.61 130.67 o 17 1 -13 72.17 -123.56 123.56 o 19 1 -13 128.93 150.17 161.08 o 21 1 -13 883.01 989.54 379.20 o 23 1 -13 89.63 346.78 652.76 o -16 2 -13 54.87 -64.30 230.61 o -14 2 -13 370.40 271.28 206.72 o -12 2 -13 460.00 629.58 152.78 o -10 2 -13 30.91 -5.12 104.73 o -8 2 -13 984.63 996.93 155.47 o -6 2 -13 274.89 228.14 117.97 o -4 2 -13 220.11 325.01 179.20 o -2 2 -13 387.92 486.06 148.61 o 0 2 -13 253.14 70.82 186.50 o 2 2 -13 424.83 392.46 194.16 o 4 2 -13 806.01 760.50 156.43 o 6 2 -13 1240.71 1143.57 188.12 o 8 2 -13 285.33 543.34 152.54 o 10 2 -13 2130.54 1542.88 293.34 o 12 2 -13 374.73 350.36 125.70 o 14 2 -13 851.48 869.32 146.70 o 16 2 -13 283.69 26.94 212.22 o 18 2 -13 613.28 560.97 180.70 o 20 2 -13 210.65 226.98 166.43 o 22 2 -13 374.47 504.66 247.36 o -15 3 -13 75.15 70.17 158.70 o -13 3 -13 153.15 -76.49 148.44 o -11 3 -13 368.67 319.10 148.38 o -9 3 -13 90.42 188.72 135.28 o -7 3 -13 283.81 166.94 126.57 o -5 3 -13 192.13 129.38 104.88 o -3 3 -13 366.65 416.62 142.51 o -1 3 -13 193.55 113.37 204.87 o 1 3 -13 18.83 -9.36 110.16 o 3 3 -13 227.97 -19.12 108.75 o 5 3 -13 814.10 685.63 157.48 o 7 3 -13 974.44 885.58 322.63 o 9 3 -13 12.73 59.11 125.59 o 11 3 -13 233.63 154.02 114.37 o 13 3 -13 1681.31 1754.40 212.69 o 15 3 -13 130.03 31.14 134.40 o 17 3 -13 224.10 283.78 152.66 o 19 3 -13 290.28 144.83 163.53 o 21 3 -13 75.50 262.91 192.01 o -14 4 -13 187.59 279.64 171.27 o -12 4 -13 8.16 32.67 146.98 o -10 4 -13 395.72 300.07 215.57 o -8 4 -13 2989.77 3102.10 352.45 o -6 4 -13 166.24 189.01 115.77 o -4 4 -13 128.96 388.65 125.88 o -2 4 -13 86.68 56.37 201.43 o 0 4 -13 263.34 150.62 141.12 o 2 4 -13 9.83 109.99 123.28 o 4 4 -13 1758.94 1661.31 232.11 o 6 4 -13 106.09 -69.79 118.12 o 8 4 -13 84.70 101.86 212.27 o 10 4 -13 149.59 300.15 118.41 o 12 4 -13 691.27 449.63 189.09 o 14 4 -13 330.32 213.79 183.35 o 16 4 -13 63.58 77.64 143.93 o 18 4 -13 455.79 296.85 176.13 o 20 4 -13 70.22 106.83 173.39 o 22 4 -13 45.96 661.21 375.15 o -13 5 -13 47.67 357.40 172.11 o -11 5 -13 151.34 554.20 197.07 o -9 5 -13 1371.14 1434.37 246.36 o -7 5 -13 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