Acta Crystallographica Section E

Structure Reports Online

Volume 69, Part 10 (October 2013)

metal-organic compounds

Acta Cryst. (2013). E69, m562-m563    [ doi:10.1107/S1600536813026172 ]

Tetra­butyl­ammonium butyl­tetra­chlorido­stannate(IV)

T. Diop, A. van der Lee and L. Diop

Abstract: In the title compound, [N(C4H9)4][Sn(C4H9)Cl4], the SnIV atom of the stannate anion has a trigonal-bipyramidal coordination sphere by two Cl atoms and one butyl chain in the equatorial plane and by two Cl atoms in the apical positions. Two of the four butyl chains of the tetra­butyl­ammonium cation are partially disordered, each with refined site occupancies of 0.691 (6):0.309 (6). Weak C-H...Cl hydrogen-bonding inter­actions help to consolidate the crystal packing, as well as a short Cl...Cl inter­action of 3.295 (2) Å.

CCDC reference: 962599

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