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[Contents scheme]

Acta Cryst. (2013). E69, m562-m563
[ doi:10.1107/S1600536813026172 ]

Tetrabutylammonium butyltetrachloridostannate(IV)

T. Diop, A. van der Lee and L. Diop


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT213_ALERT_2_B Atom C18 has ADP max/min Ratio ..... 4.2 prola PLAT220_ALERT_2_B Large Non-Solvent C Ueq(max)/Ueq(min) ... 5.0 Ratio
Alert level C PLAT213_ALERT_2_C Atom C17 has ADP max/min Ratio ..... 3.5 prola PLAT222_ALERT_3_C Large Non-Solvent H Uiso(max)/Uiso(min) .. 6.5 Ratio PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C25 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for N10 PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of Sn1 PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.7 PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0111 Ang. PLAT410_ALERT_2_C Short Intra H...H Contact H201 .. H113 .. 1.92 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H191 .. CL5 .. 2.88 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H192 .. CL5 .. 2.90 Ang. PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 4
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C12 PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C24 PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C241 PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 12 % PLAT434_ALERT_2_G Short Inter HL..HL Contact Cl2 .. Cl2 . 3.30 Ang. PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 4 PLAT808_ALERT_5_G No Parseable SHELXL Style Weighting Scheme Found ! Check PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 142 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 925 PLAT929_ALERT_5_G No Weight Pars,Obs and Calc R1,wR2,S not checked ! Info PLAT960_ALERT_3_G Number of Intensities with I < - 2*sig(I) ... 32
0 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 11 ALERT level C = Check. Ensure it is not caused by an omission or oversight 12 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 11 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 5 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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