[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m590
[ doi:10.1107/S1600536813026160 ]

[2,6-Di­fluoro-3-(pyridin-2-yl-[kappa]N)pyridin-4-yl-[kappa]C4](penta­ne-2,4-dionato-[kappa]2O,O')iridium(III)

K. Luo, C. Zhang, J. Jia and D. Luo


Key indicators

checkCIF/PLATON results

No syntax errors found



Alert level A PLAT726_ALERT_2_A H...A Calc 2.30000, Rep 2.36000 Dev... 0.06 Ang. H4 -F2 1.555 1.555 # 59
Alert level C PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.506 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 7
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT128_ALERT_4_G Note: Alternate Setting of Space-group P21/c . P21/n PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 20 O1 -IR1 -C17 -C16 -4.00 2.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 21 O1 -IR1 -C17 -C18 173.00 2.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 28 O2 -IR1 -C7 -C6 -11.00 2.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 29 O2 -IR1 -C7 -C8 165.30 1.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 34 N1 -IR1 -N3 -C11 138.50 1.40 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 35 N1 -IR1 -N3 -C15 -38.20 1.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 45 N3 -IR1 -N1 -C1 119.50 1.40 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 46 N3 -IR1 -N1 -C5 -55.70 1.50 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 69 C7 -IR1 -O2 -C23 -76.00 1.90 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 100 C17 -IR1 -O1 -C21 -78.00 2.00 1.555 1.555 1.555 1.555
1 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 2 ALERT level C = Check. Ensure it is not caused by an omission or oversight 14 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 11 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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