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[Contents scheme]

Acta Cryst. (2013). E69, o1617-o1618
[ doi:10.1107/S160053681302713X ]

N-[2-(2,2-Di­methyl­propanamido)­pyrimidin-4-yl]-2,2-di­methyl­propanamide n-hexane 0.25-solvate hemihydrate

B. Osmialowski, A. Valkonen and L. Checinska


Key indicators

checkCIF/PLATON results

No syntax errors found



Datablock: I



Alert level C PLAT242_ALERT_2_C Low Ueq as Compared to Neighbors for ..... C9 Check PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0057 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 5.860 Check PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.945 Check PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 5 Why ? PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 36
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 22 Note PLAT003_ALERT_2_G Number of Uiso or Uij Restrained non-H Atoms ... 11 PLAT301_ALERT_3_G Main Residue Disorder ............ Percentage = 8 Note PLAT302_ALERT_4_G Anion/Solvent Disorder ............ Percentage = 29 Note PLAT860_ALERT_3_G Number of Least-Squares Restraints ............. 101 Note
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 7 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check

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