[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o1714
[ doi:10.1107/S1600536813028845 ]

6,6'-Dieth­oxy-2,2'-[4-methyl-1,2-phenyl­enebis(nitrilo­methanylyl­idene)]diphenol aceto­nitrile monosolvate

L. Li and S. Zeng


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C RINTA01_ALERT_3_C The value of Rint is greater than 0.12 Rint given 0.122 PLAT230_ALERT_2_C Hirshfeld Test Diff for C22 -- C25 .. 6.0 su PLAT234_ALERT_4_C Large Hirshfeld Difference C5 -- C6 .. 0.16 Ang. PLAT234_ALERT_4_C Large Hirshfeld Difference C8 -- C9 .. 0.19 Ang. PLAT241_ALERT_2_C High Ueq as Compared to Neighbors for ..... C13 Check PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C27 Check PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0080 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 32.777 Check PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 8.283 Check PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.806 Check PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.091 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 11
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT007_ALERT_5_G Number of Unrefined Donor-H Atoms .............. 2 Why ? PLAT199_ALERT_1_G Reported _cell_measurement_temperature ..... (K) 293 Check PLAT200_ALERT_1_G Reported _diffrn_ambient_temperature ..... (K) 293 Check PLAT910_ALERT_3_G Missing # of FCF Reflections Below Th(Min) ..... 1 Why ?
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 12 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 8 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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