[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m605-m606
[ doi:10.1107/S160053681302583X ]

Ethyl­enedi­ammonium sodium tetra­kis­[bis­(ethyl­enedi­amine-[kappa]2N,N')(oxalato-[kappa]2O1,O2)cobalt(III)] [penta­hydrogen di(phosphato­octa­deca­tungstate)] tetra­deca­hydrate

S. Zhang, J. Wang and Y. Xu


Key indicators

checkCIF/PLATON results

No syntax errors found



Datablock: 1


Alert level A PLAT900_ALERT_1_A No Matching Reflection File Found .............. Please Check
Alert level C PLAT068_ALERT_1_C Reported F000 Differs from Calcd (or Missing)... Please Check PLAT213_ALERT_2_C Atom O27 has ADP max/min Ratio ..... 3.2 oblate PLAT234_ALERT_4_C Large Hirshfeld Difference O63 -- C2 .. 0.16 Ang. PLAT234_ALERT_4_C Large Hirshfeld Difference C3 -- C4 .. 0.18 Ang. PLAT241_ALERT_2_C High Ueq as Compared to Neighbors for ..... C4 Check PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0190 Ang. PLAT417_ALERT_2_C Short Inter D-H..H-D H2WB .. H6WD .. 2.11 Ang. PLAT420_ALERT_2_C D-H Without Acceptor N3 - H3D ... Please Check PLAT420_ALERT_2_C D-H Without Acceptor N10 - H10D ... Please Check PLAT924_ALERT_1_C The Reported and Calculated Rho(min) Differ by . 1.98 eA-3
Alert level G FORMU01_ALERT_1_G There is a discrepancy between the atom counts in the _chemical_formula_sum and _chemical_formula_moiety. This is usually due to the moiety formula being in the wrong format. Atom count from _chemical_formula_sum: C26 H102 Co4 N18 Na1 O154 P Atom count from _chemical_formula_moiety:C26 H107 Co4 N18 Na1 O154 P PLAT003_ALERT_2_G Number of Uiso or Uij Restrained non-H Atoms ... 2 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT007_ALERT_5_G Number of Unrefined Donor-H Atoms .............. 33 Why ? PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ Please Check PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00200 Deg. PLAT199_ALERT_1_G Reported _cell_measurement_temperature ..... (K) 293 Check PLAT200_ALERT_1_G Reported _diffrn_ambient_temperature ..... (K) 293 Check PLAT605_ALERT_4_G Structure Contains Solvent Accessible VOIDS of . 614 A   3 PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 14 PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 2 C6 H16 Co N4 O4 PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 5 H2 O PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 6 H2 O PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 7 H2 O PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 8 H2 O PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 10 H2 O PLAT793_ALERT_4_G The Model has Chirality at P1 (Verify) R PLAT793_ALERT_4_G The Model has Chirality at P2 (Verify) S PLAT860_ALERT_3_G Number of Least-Squares Restraints ............. 12 Note PLAT869_ALERT_4_G ALERTS Related to the use of SQUEEZE Suppressed ! Info
1 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 10 ALERT level C = Check. Ensure it is not caused by an omission or oversight 20 ALERT level G = General information/check it is not something unexpected 8 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 13 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster