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[Contents scheme]

Acta Cryst. (2013). E69, o1615
[ doi:10.1107/S1600536813027037 ]

4-Amino-N-(4,6-di­methyl­pyrimidin-2-yl)benzene­sulfonamide-1,4-di­aza­bicyclo­[2.2.2]octane (2/1)

H. D. Arman, T. Kaulgud and E. R. T. Tiekink


Key indicators

checkCIF/PLATON results

No syntax errors found



Alert level A DIFF020_ALERT_1_A _diffrn_standards_interval_count and _diffrn_standards_interval_time are missing. Number of measurements between standards or time (min) between standards.
Alert level C PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.879 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 17 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1 PLAT975_ALERT_2_C Positive Residual Density at 0.92A from N5 . 0.45 eA-3 PLAT976_ALERT_2_C Negative Residual Density at 1.05A from N1 . -0.41 eA-3
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 5 Note PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT860_ALERT_3_G Number of Least-Squares Restraints ............. 3 Note PLAT910_ALERT_3_G Missing # of FCF Reflections Below Th(Min) ..... 1 Why ? PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 7
1 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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