[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o1815
[ doi:10.1107/S1600536813031516 ]

N-(Adamantan-1-yl)-1,2,3,4-tetra­hydro­iso­quinoline-2-carbo­thio­amide

A. A. El-Emam, E. S. Al-Abdullah, H. M. Al-Tuwaijri, C. S. Chidan Kumar and H.-K. Fun


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C THETM01_ALERT_3_C The value of sine(theta_max)/wavelength is less than 0.590 Calculated sin(theta_max)/wavelength = 0.5878 PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.970 PLAT420_ALERT_2_C D-H Without Acceptor N2 - H1N2 ... Please Check PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.192 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.588 87
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size .... 0.81 mm PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 1 PLAT793_ALERT_4_G The Model has Chirality at C11 (Verify) S PLAT793_ALERT_4_G The Model has Chirality at C13 (Verify) S PLAT793_ALERT_4_G The Model has Chirality at C18 (Verify) S PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 59 % PLAT910_ALERT_3_G Missing # of FCF Reflections Below Th(Min) ..... 1 Why ? PLAT960_ALERT_3_G Number of Intensities with I < - 2*sig(I) ... 1
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 9 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 7 ALERT type 3 Indicator that the structure quality may be low 5 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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