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Acta Cryst. (2013). E69, m651
[ doi:10.1107/S1600536813030432 ]

([mu]3-Hydrido)[[mu]3-2-(tri­methyl­sil­yl)ethyl­idyne-[kappa]3C1:C1:C1]tetra­kis­[([eta]5-cyclo­penta­dien­yl)cobalt(II)]

M. Haehnel, A. Spannenberg and U. Rosenthal


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT213_ALERT_2_C Atom C15 has ADP max/min Ratio ..... 3.5 prolat PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.7 Ratio PLAT241_ALERT_2_C High Ueq as Compared to Neighbors for ..... C15 Check PLAT242_ALERT_2_C Low Ueq as Compared to Neighbors for ..... Co2 Check PLAT242_ALERT_2_C Low Ueq as Compared to Neighbors for ..... Co3 Check PLAT242_ALERT_2_C Low Ueq as Compared to Neighbors for ..... Co4 Check PLAT731_ALERT_1_C Bond Calc 1.391(4), Rep 1.3914(15) ...... 3 su-Rat C14 -C15 1.555 1.555 # 45 PLAT731_ALERT_1_C Bond Calc 1.394(3), Rep 1.3942(14) ...... 2 su-Rat C21 -C22 1.555 1.555 # 65 PLAT731_ALERT_1_C Bond Calc 1.394(3), Rep 1.3942(14) ...... 2 su-Rat C21 -C25 1.555 1.555 # 66 PLAT731_ALERT_1_C Bond Calc 1.394(3), Rep 1.3942(14) ...... 2 su-Rat C22 -C23 1.555 1.555 # 69 PLAT731_ALERT_1_C Bond Calc 1.394(3), Rep 1.3942(14) ...... 2 su-Rat C23 -C24 1.555 1.555 # 72 PLAT731_ALERT_1_C Bond Calc 1.394(3), Rep 1.3942(14) ...... 2 su-Rat C24 -C25 1.555 1.555 # 75
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT303_ALERT_2_G Full Occupancy H-Atom H1 with # Connections 3.00 Check PLAT343_ALERT_2_G Check sp? Angle Range in Main Residue for .. C1 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 319 Do ! C18 -C19 -CO3 -CO2 -67.40 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 320 Do ! C20 -C19 -CO3 -CO2 174.40 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 363 Do ! C20 -C16 -CO3 -CO4 133.50 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 364 Do ! C17 -C16 -CO3 -CO4 15.00 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 423 Do ! C1 -CO2 -CO3 -C19 -59.70 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 424 Do ! C11 -CO2 -CO3 -C19 61.50 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 425 Do ! C15 -CO2 -CO3 -C19 72.70 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 426 Do ! C12 -CO2 -CO3 -C19 146.60 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 427 Do ! C14 -CO2 -CO3 -C19 109.60 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 428 Do ! C13 -CO2 -CO3 -C19 143.20 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 429 Do ! CO4 -CO2 -CO3 -C19 -23.80 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 430 Do ! CO1 -CO2 -CO3 -C19 -93.70 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 567 Do ! C21 -C22 -CO4 -CO2 170.30 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 568 Do ! C23 -C22 -CO4 -CO2 -71.10 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 573 Do ! C16 -CO3 -CO4 -C1 120.90 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 580 Do ! C16 -CO3 -CO4 -C24 -12.10 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 587 Do ! C16 -CO3 -CO4 -C25 -30.30 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 594 Do ! C16 -CO3 -CO4 -C23 -96.40 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 601 Do ! C16 -CO3 -CO4 -C21 -68.70 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 608 Do ! C16 -CO3 -CO4 -C22 -101.10 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 615 Do ! C16 -CO3 -CO4 -CO1 156.70 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 621 Do ! C16 -CO3 -CO4 -CO2 84.80 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 723 Do ! C1 -CO2 -CO4 -C22 15.70 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 724 Do ! C11 -CO2 -CO4 -C22 100.70 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 725 Do ! C15 -CO2 -CO4 -C22 142.00 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 726 Do ! C12 -CO2 -CO4 -C22 73.70 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 727 Do ! C14 -CO2 -CO4 -C22 177.60 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 728 Do ! C13 -CO2 -CO4 -C22 -178.00 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 729 Do ! CO3 -CO2 -CO4 -C22 -114.50 0.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 730 Do ! CO1 -CO2 -CO4 -C22 -44.20 0.60 1.555 1.555 1.555 1.555 PLAT764_ALERT_4_G Overcomplete CIF Bond List Detected (Rep/Expd) . 1.13 Ratio PLAT960_ALERT_3_G Number of Intensities with I < - 2*sig(I) ... 2
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 12 ALERT level C = Check. Ensure it is not caused by an omission or oversight 35 ALERT level G = General information/check it is not something unexpected 6 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 8 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 31 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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