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[Contents scheme]

Acta Cryst. (2013). E69, m683
[ doi:10.1107/S1600536813031838 ]

Bis{[mu]4-N-[phen­yl(pyridin-2-yl­aza­nid­yl)meth­yl]pyridin-2-aminido}tetra­kis(tetra­hydro­furan)­tetra­lithium

J. Chen


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT234_ALERT_4_C Large Hirshfeld Difference C4 -- C5 .. 0.17 Ang. PLAT241_ALERT_2_C High Ueq as Compared to Neighbors for ..... C11 Check PLAT243_ALERT_4_C High 'Solvent' Ueq as Compared to Neighbors of C18 Check PLAT243_ALERT_4_C High 'Solvent' Ueq as Compared to Neighbors of C20 Check PLAT243_ALERT_4_C High 'Solvent' Ueq as Compared to Neighbors of C21 Check PLAT243_ALERT_4_C High 'Solvent' Ueq as Compared to Neighbors of C22 Check PLAT243_ALERT_4_C High 'Solvent' Ueq as Compared to Neighbors of C24 Check PLAT243_ALERT_4_C High 'Solvent' Ueq as Compared to Neighbors of C25 Check PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of O1 Check PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of O2 Check PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0092 Ang. PLAT360_ALERT_2_C Short C(sp3)-C(sp3) Bond C18 - C19 ... 1.39 Ang. PLAT360_ALERT_2_C Short C(sp3)-C(sp3) Bond C19 - C20 ... 1.35 Ang. PLAT360_ALERT_2_C Short C(sp3)-C(sp3) Bond C22 - C23 ... 1.42 Ang. PLAT360_ALERT_2_C Short C(sp3)-C(sp3) Bond C23 - C24 ... 1.35 Ang. PLAT360_ALERT_2_C Short C(sp3)-C(sp3) Bond C24 - C25 ... 1.37 Ang. PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -1.777 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.594 20
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 2 Note PLAT003_ALERT_2_G Number of Uiso or Uij Restrained non-H Atoms ... 10 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ Please Check PLAT045_ALERT_1_G Calculated and Reported Z Differ by ............ 2.00 Ratio PLAT072_ALERT_2_G SHELXL First Parameter in WGHT Unusually Large. 0.15 PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00200 Deg. PLAT764_ALERT_4_G Overcomplete CIF Bond List Detected (Rep/Expd) . 1.64 Ratio PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 5 Li PLAT860_ALERT_3_G Number of Least-Squares Restraints ............. 61 Note
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 18 ALERT level C = Check. Ensure it is not caused by an omission or oversight 10 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 9 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 11 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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