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Acta Cryst. (2013). E69, o1844-o1845  [ doi:10.1107/S1600536813032042 ]

Dimethyl (2Z)-2-[4-((1Z)-1-{2-[(2Z,5Z)-5-(2-meth­oxy-2-oxo­ethyl­idene)-4-oxo-3-phenyl-1,3-thia­zolidin-2-yl­idene]hydra­zin-1-yl­idene}eth­yl)anilino]but-2-ene­dio­ate

S. K. Mohamed, M. Akkurt, J. T. Mague, A. A. Hassan and M. R. Albayati


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Alert level B THETM01_ALERT_3_B The value of sine(theta_max)/wavelength is less than 0.575 Calculated sin(theta_max)/wavelength = 0.5563 PLAT019_ALERT_1_B Check _diffrn_measured_fraction_theta_full/_max 0.802 PLAT023_ALERT_3_B Resolution (too) Low [sin(theta)/Lambda < 0.6].. 59.06 Deg.
Alert level C PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0070 Ang. PLAT413_ALERT_2_C Short Inter XH3 .. XHn H14C .. H12A .. 2.05 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 6.817 Check PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.426 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.556 52
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 3 Note PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT007_ALERT_5_G Number of Unrefined Donor-H Atoms .............. 1 Why ? PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 6.49 PLAT301_ALERT_3_G Main Residue Disorder ............ Percentage = 16 Note PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... ! Info PLAT860_ALERT_3_G Number of Least-Squares Restraints ............. 6 Note PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 44 %
0 ALERT level A = Most likely a serious problem - resolve or explain 3 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 8 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 9 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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