# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' ' _shelx_refln_list_code 4 _shelx_F_calc_maximum 104.26 _exptl_crystal_F_000 336.00 _reflns_d_resolution_high 0.7003 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 9.3031 _cell_length_b 5.8892 _cell_length_c 9.7620 _cell_angle_alpha 90.000 _cell_angle_beta 96.111 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10869.45 9285.18 23.12 o 4 0 0 2096.77 2297.15 11.62 o 6 0 0 1407.03 1492.98 8.35 o 8 0 0 7.56 8.96 1.58 o 10 0 0 385.36 393.38 8.84 o 12 0 0 707.54 684.75 15.18 o 1 1 0 7933.11 5848.94 19.65 o 2 1 0 1692.75 1976.26 16.87 o 3 1 0 138.57 180.87 2.71 o 4 1 0 186.80 202.79 2.29 o 5 1 0 2036.02 2106.14 26.05 o 6 1 0 133.97 140.09 3.86 o 7 1 0 118.79 136.37 1.54 o 8 1 0 786.78 792.33 12.23 o 9 1 0 44.17 49.52 1.15 o 10 1 0 1035.85 1081.13 12.08 o 11 1 0 236.93 241.28 4.04 o 12 1 0 127.65 124.17 2.77 o 13 1 0 323.12 282.46 6.16 o 0 2 0 134.21 151.02 3.75 o 1 2 0 1047.25 986.58 51.17 o 2 2 0 566.65 689.25 20.20 o 3 2 0 240.63 223.05 2.26 o 4 2 0 559.14 575.10 7.59 o 5 2 0 1090.94 1069.55 23.48 o 6 2 0 1333.69 1398.54 11.54 o 7 2 0 487.91 517.20 4.45 o 8 2 0 431.14 451.64 7.05 o 9 2 0 372.89 395.17 3.98 o 10 2 0 282.36 269.26 20.92 o 11 2 0 61.54 62.51 2.01 o 12 2 0 26.11 22.83 2.36 o 1 3 0 1069.81 999.27 35.06 o 2 3 0 76.66 79.21 5.33 o 3 3 0 2988.66 2715.26 156.06 o 4 3 0 4.59 11.37 2.11 o 5 3 0 2493.62 2467.69 38.40 o 6 3 0 913.13 874.73 28.88 o 7 3 0 1660.57 1708.06 19.40 o 8 3 0 9.32 12.03 1.08 o 9 3 0 1749.17 1723.46 67.34 o 10 3 0 0.00 3.44 1.03 o 11 3 0 345.64 338.45 4.10 o 12 3 0 32.85 23.71 2.05 o 0 4 0 42.62 42.62 1.73 o 1 4 0 49.42 46.05 1.30 o 2 4 0 1415.94 1375.13 26.02 o 3 4 0 321.38 323.59 3.95 o 4 4 0 2172.37 2152.72 34.68 o 5 4 0 83.59 86.85 4.84 o 6 4 0 889.84 907.58 9.68 o 7 4 0 67.29 69.54 1.86 o 8 4 0 1399.05 1397.94 24.12 o 9 4 0 99.52 97.97 1.18 o 10 4 0 710.88 709.61 6.78 o 11 4 0 66.27 66.08 2.82 o 1 5 0 90.61 84.50 1.44 o 2 5 0 225.55 222.87 1.90 o 3 5 0 477.17 505.19 6.41 o 4 5 0 668.33 655.96 10.27 o 5 5 0 151.75 157.45 1.44 o 6 5 0 102.41 101.67 3.52 o 7 5 0 194.74 201.62 2.88 o 8 5 0 22.05 22.89 3.00 o 9 5 0 214.52 220.04 3.29 o 10 5 0 202.54 192.21 6.17 o 0 6 0 585.56 576.91 7.89 o 1 6 0 35.84 36.55 1.04 o 2 6 0 969.83 925.53 31.33 o 3 6 0 278.73 279.20 6.32 o 4 6 0 230.84 222.34 10.58 o 5 6 0 38.45 39.28 3.73 o 6 6 0 7.12 7.08 1.20 o 7 6 0 30.54 33.65 1.17 o 8 6 0 27.61 32.15 1.78 o 9 6 0 302.47 281.64 11.67 o 1 7 0 2042.21 2028.64 25.56 o 2 7 0 15.07 20.17 1.53 o 3 7 0 746.38 760.82 11.64 o 4 7 0 9.16 8.94 1.38 o 5 7 0 19.04 19.72 1.16 o 6 7 0 2.36 3.49 1.29 o 7 7 0 7.83 5.19 1.31 o 0 8 0 252.78 226.78 16.28 o 1 8 0 64.62 66.90 4.18 o 2 8 0 180.85 180.87 5.96 o 3 8 0 180.35 162.97 7.59 o 4 8 0 19.38 10.23 1.59 o -13 0 1 42.26 35.38 4.98 o -11 0 1 185.08 191.42 4.88 o -9 0 1 1966.87 2022.05 53.22 o -7 0 1 5211.02 4803.94 270.15 o -5 0 1 4181.59 4076.85 73.91 o -3 0 1 2129.46 2383.17 103.02 o -1 0 1 27.79 38.10 5.57 o 1 0 1 129.80 131.44 9.66 o 3 0 1 214.63 249.50 2.31 o 5 0 1 5140.30 5017.88 32.40 o 7 0 1 7943.91 7927.01 12.27 o 9 0 1 377.94 417.59 11.97 o 11 0 1 315.83 319.50 3.63 o 13 0 1 14.12 8.58 1.96 o -13 1 1 54.04 50.97 2.23 o -12 1 1 154.12 155.36 2.02 o -11 1 1 81.66 81.18 1.50 o -10 1 1 469.80 463.47 24.40 o -9 1 1 68.06 72.39 1.13 o -8 1 1 2283.08 2309.04 40.27 o -7 1 1 128.03 134.17 2.78 o -6 1 1 1328.23 1331.48 9.57 o -5 1 1 204.60 231.75 2.20 o -4 1 1 975.40 999.81 10.69 o -3 1 1 5615.72 5389.13 93.95 o -2 1 1 641.49 695.97 37.11 o -1 1 1 275.77 339.90 5.85 o 0 1 1 1379.94 1363.25 8.82 o 1 1 1 1420.50 1590.97 32.62 o 2 1 1 1781.87 2012.75 88.80 o 3 1 1 501.48 564.97 16.27 o 4 1 1 463.91 441.50 2.40 o 5 1 1 1304.43 1375.27 13.07 o 6 1 1 4971.88 4864.91 54.33 o 7 1 1 43.78 46.27 1.42 o 8 1 1 955.56 1013.92 14.95 o 9 1 1 555.32 582.22 5.64 o 10 1 1 135.08 143.44 3.05 o 11 1 1 348.34 354.17 3.43 o 12 1 1 348.81 341.68 5.32 o -12 2 1 410.83 399.66 9.97 o -11 2 1 177.15 178.49 3.17 o -10 2 1 66.20 72.14 2.53 o -9 2 1 308.45 308.74 8.48 o -8 2 1 0.01 -0.08 0.93 o -7 2 1 318.42 316.24 4.15 o -6 2 1 55.11 57.01 1.35 o -5 2 1 10.71 12.92 1.14 o -4 2 1 1757.56 1811.12 22.03 o -3 2 1 1830.97 1796.01 25.16 o -2 2 1 1429.45 1437.18 20.32 o -1 2 1 2321.52 2263.00 76.53 o 0 2 1 3692.81 3404.69 43.79 o 1 2 1 5911.19 5413.99 248.52 o 2 2 1 131.85 118.50 3.49 o 3 2 1 2480.88 2536.43 27.40 o 4 2 1 179.87 172.05 1.59 o 5 2 1 291.29 290.50 6.39 o 6 2 1 424.02 432.73 8.09 o 7 2 1 317.11 309.55 5.05 o 8 2 1 187.17 186.62 3.68 o 9 2 1 42.13 42.15 1.76 o 10 2 1 114.98 109.98 5.75 o 11 2 1 415.15 419.96 5.44 o 12 2 1 176.15 164.37 8.68 o -12 3 1 294.19 265.24 18.16 o -11 3 1 30.33 32.02 1.49 o -10 3 1 7.41 8.39 1.18 o -9 3 1 1.28 2.27 1.37 o -8 3 1 55.98 59.51 1.41 o -7 3 1 26.59 22.18 2.12 o -6 3 1 112.76 114.83 1.95 o -5 3 1 5.85 7.62 1.17 o -4 3 1 2249.59 2130.91 32.32 o -3 3 1 469.68 456.93 11.68 o -2 3 1 5095.72 4533.56 138.32 o -1 3 1 142.64 134.48 3.59 o 0 3 1 1843.66 1586.38 28.31 o 1 3 1 921.81 806.97 60.35 o 2 3 1 3445.99 3080.09 56.21 o 3 3 1 418.27 459.37 5.77 o 4 3 1 614.31 576.71 16.27 o 5 3 1 126.82 116.62 3.00 o 6 3 1 5.22 5.97 1.99 o 7 3 1 1.62 4.77 1.36 o 8 3 1 82.47 83.86 1.83 o 9 3 1 8.38 9.37 0.98 o 10 3 1 265.57 266.25 5.47 o 11 3 1 0.02 1.75 1.57 o 12 3 1 304.33 280.92 10.03 o -11 4 1 86.24 79.19 4.73 o -10 4 1 24.67 26.77 2.04 o -9 4 1 8.28 10.33 1.06 o -8 4 1 8.99 9.76 1.50 o -7 4 1 26.09 27.71 1.66 o -6 4 1 142.91 151.25 3.54 o -5 4 1 427.54 413.95 5.02 o -4 4 1 340.29 321.02 12.89 o -3 4 1 2995.78 2773.87 66.68 o -2 4 1 218.27 213.11 4.89 o -1 4 1 1831.36 1552.02 85.58 o 0 4 1 4.21 6.32 1.29 o 1 4 1 1239.50 1046.70 42.64 o 2 4 1 122.54 118.40 4.18 o 3 4 1 1653.92 1551.18 14.60 o 4 4 1 173.18 185.31 1.76 o 5 4 1 21.34 23.29 1.42 o 6 4 1 18.52 16.79 1.10 o 7 4 1 3.94 5.40 1.00 o 8 4 1 24.10 28.49 1.49 o 9 4 1 270.24 276.22 2.06 o 10 4 1 19.50 18.00 2.00 o 11 4 1 176.30 151.94 12.03 o -10 5 1 199.72 198.95 4.47 o -9 5 1 0.11 1.22 1.16 o -8 5 1 100.09 97.03 7.80 o -7 5 1 0.02 1.06 1.17 o -6 5 1 77.17 81.93 1.32 o -5 5 1 746.83 739.52 14.93 o -4 5 1 230.32 231.24 5.14 o -3 5 1 640.45 630.08 11.49 o -2 5 1 630.40 581.30 14.79 o -1 5 1 22.54 22.21 1.45 o 0 5 1 706.97 636.57 17.33 o 1 5 1 39.40 39.42 1.30 o 2 5 1 1281.78 1210.64 18.11 o 3 5 1 678.10 671.52 12.53 o 4 5 1 717.94 648.21 48.65 o 5 5 1 152.59 158.61 5.20 o 6 5 1 3.91 8.34 1.93 o 7 5 1 0.12 1.97 0.98 o 8 5 1 150.37 157.15 1.86 o 9 5 1 57.30 58.11 2.91 o 10 5 1 238.82 225.45 2.42 o -9 6 1 372.39 349.47 10.63 o -8 6 1 25.36 21.38 2.07 o -7 6 1 509.01 479.38 54.34 o -6 6 1 16.73 18.08 1.36 o -5 6 1 573.37 559.10 16.52 o -4 6 1 675.09 596.11 49.05 o -3 6 1 68.58 68.76 1.21 o -2 6 1 112.34 118.88 1.22 o -1 6 1 44.78 42.16 2.41 o 0 6 1 8.12 11.73 1.01 o 1 6 1 63.53 69.38 1.41 o 2 6 1 142.23 130.43 6.34 o 3 6 1 422.20 426.85 11.63 o 4 6 1 410.66 406.43 15.30 o 5 6 1 620.94 530.66 65.26 o 6 6 1 17.24 19.10 1.97 o 7 6 1 495.32 490.69 16.26 o 8 6 1 35.04 29.15 1.22 o 9 6 1 479.31 456.73 17.16 o -7 7 1 39.80 35.72 2.66 o -6 7 1 997.00 1022.52 24.64 o -5 7 1 6.03 9.34 1.19 o -4 7 1 328.72 334.18 10.55 o -3 7 1 6.41 6.01 1.02 o -2 7 1 4.01 8.32 1.18 o -1 7 1 43.33 46.10 1.05 o 0 7 1 4.22 5.82 1.34 o 1 7 1 4.16 0.75 1.84 o 2 7 1 14.36 15.49 1.42 o 3 7 1 5.96 8.75 2.89 o 4 7 1 335.29 358.27 8.15 o 5 7 1 3.22 3.95 1.16 o 6 7 1 823.87 826.76 19.90 o 7 7 1 0.87 1.49 1.88 o -3 8 1 2.16 0.29 1.16 o -2 8 1 87.01 88.77 1.16 o -1 8 1 75.47 76.22 1.22 o 0 8 1 0.04 1.45 1.48 o 1 8 1 62.02 58.77 2.83 o 2 8 1 154.27 152.49 1.82 o 3 8 1 35.48 32.20 2.34 o -12 0 2 37.72 34.53 2.67 o -10 0 2 198.76 215.20 2.85 o -8 0 2 185.07 198.91 4.25 o -6 0 2 14.07 15.56 1.61 o -4 0 2 128.89 110.61 2.37 o 4 0 2 4099.85 4483.97 66.79 o 6 0 2 156.17 176.27 6.22 o 8 0 2 59.22 64.02 3.33 o 10 0 2 349.73 355.72 5.74 o 12 0 2 1437.75 1428.95 45.74 o -13 1 2 104.39 93.93 2.14 o -12 1 2 36.81 35.17 1.51 o -11 1 2 379.88 396.54 3.63 o -10 1 2 394.04 397.86 4.99 o -9 1 2 119.24 125.79 3.22 o -8 1 2 118.41 121.67 1.74 o -7 1 2 117.49 119.62 2.50 o -6 1 2 1.22 1.32 1.02 o -5 1 2 1742.30 1717.75 44.39 o -4 1 2 899.81 1024.91 16.45 o -3 1 2 3857.61 3797.91 87.59 o -2 1 2 156.13 152.22 4.36 o 0 1 2 248.09 240.17 16.73 o 1 1 2 1242.92 1239.11 28.52 o 2 1 2 8945.00 8671.11 16.42 o 3 1 2 1151.94 1319.05 10.16 o 4 1 2 5067.52 5458.31 20.86 o 5 1 2 417.71 458.49 9.45 o 6 1 2 310.92 340.96 10.38 o 7 1 2 57.44 66.23 4.02 o 8 1 2 5.23 8.28 1.07 o 9 1 2 183.51 194.27 3.35 o 10 1 2 144.39 142.81 9.17 o 11 1 2 271.66 271.49 3.97 o 12 1 2 201.59 197.19 3.88 o -12 2 2 307.14 305.25 1.47 o -11 2 2 272.10 279.66 3.41 o -10 2 2 672.29 693.10 9.29 o -9 2 2 146.00 145.06 2.12 o -8 2 2 920.55 913.05 42.14 o -7 2 2 1685.61 1591.80 66.10 o -6 2 2 2822.69 2819.15 27.66 o -5 2 2 1244.74 1238.70 15.86 o -4 2 2 2309.90 2415.11 35.32 o -3 2 2 358.79 356.98 5.26 o -2 2 2 3918.97 3775.98 120.98 o -1 2 2 2244.88 2068.44 63.09 o 0 2 2 721.71 705.28 17.37 o 1 2 2 83.27 89.94 2.07 o 2 2 2 6.16 6.53 1.53 o 3 2 2 1561.32 1450.29 35.73 o 4 2 2 1072.75 1114.17 9.67 o 5 2 2 10.29 9.79 1.29 o 6 2 2 435.76 468.20 7.07 o 7 2 2 550.00 516.08 29.82 o 8 2 2 682.57 674.17 39.14 o 9 2 2 85.56 88.71 2.00 o 10 2 2 174.07 179.17 1.36 o 11 2 2 205.30 212.98 3.96 o 12 2 2 8.15 10.17 1.10 o -12 3 2 5.15 3.94 1.30 o -11 3 2 315.46 308.54 4.02 o -10 3 2 169.19 166.70 2.36 o -9 3 2 940.22 964.11 9.60 o -8 3 2 213.57 221.77 2.03 o -7 3 2 2054.66 2107.19 19.37 o -6 3 2 1242.05 1234.16 27.39 o -5 3 2 420.20 439.90 5.44 o -4 3 2 81.18 81.69 1.41 o -3 3 2 27.22 24.29 1.43 o -2 3 2 795.86 803.28 17.65 o -1 3 2 129.67 135.51 2.77 o 0 3 2 244.14 232.74 9.61 o 1 3 2 302.65 295.05 3.95 o 2 3 2 1.77 5.90 1.17 o 3 3 2 3204.33 3060.82 66.10 o 4 3 2 10.58 27.15 2.33 o 5 3 2 2969.36 2987.84 18.29 o 6 3 2 472.83 486.63 5.38 o 7 3 2 1511.59 1539.72 18.71 o 8 3 2 93.65 99.79 1.44 o 9 3 2 1166.93 1122.99 42.49 o 10 3 2 9.72 11.00 1.09 o 11 3 2 91.57 88.37 1.36 o -11 4 2 51.72 47.95 4.21 o -10 4 2 287.21 286.54 3.22 o -9 4 2 39.62 38.00 1.14 o -8 4 2 1172.02 1191.19 11.27 o -7 4 2 86.03 82.13 3.43 o -6 4 2 1091.22 1111.09 18.97 o -5 4 2 1315.78 1224.81 40.14 o -4 4 2 22.01 24.18 1.29 o -3 4 2 425.06 381.37 33.22 o -2 4 2 3.72 7.14 1.63 o -1 4 2 62.16 60.14 1.39 o 0 4 2 83.20 86.34 3.00 o 1 4 2 32.09 94.17 30.67 o 2 4 2 916.65 898.09 11.25 o 3 4 2 0.08 0.36 1.18 o 4 4 2 2372.67 2166.78 111.90 o 5 4 2 270.97 250.74 2.58 o 6 4 2 1391.04 1438.18 14.33 o 7 4 2 40.80 42.48 1.24 o 8 4 2 1184.42 1097.84 60.31 o 9 4 2 196.79 203.40 1.81 o 10 4 2 408.42 402.24 4.91 o 11 4 2 39.73 33.01 2.06 o -10 5 2 92.64 86.42 4.58 o -9 5 2 181.57 171.75 9.94 o -8 5 2 0.11 0.30 1.72 o -7 5 2 745.78 747.81 19.06 o -6 5 2 603.10 610.94 8.91 o -5 5 2 980.85 949.87 48.96 o -4 5 2 703.32 657.99 35.13 o -3 5 2 913.26 906.05 14.76 o -2 5 2 44.89 46.13 2.45 o -1 5 2 489.43 459.02 9.08 o 0 5 2 69.71 66.91 1.65 o 1 5 2 217.89 224.41 5.89 o 2 5 2 735.69 709.00 12.95 o 3 5 2 150.38 159.67 2.45 o 4 5 2 151.29 146.31 3.86 o 5 5 2 137.69 144.83 6.45 o 6 5 2 49.53 54.48 1.59 o 7 5 2 249.01 251.47 4.58 o 8 5 2 43.99 49.69 1.51 o 9 5 2 231.68 222.89 9.42 o 10 5 2 255.29 240.89 6.16 o -9 6 2 96.41 94.39 2.69 o -8 6 2 12.19 12.32 1.23 o -7 6 2 19.35 21.36 1.16 o -6 6 2 88.06 93.86 1.21 o -5 6 2 18.12 20.17 1.57 o -4 6 2 644.04 663.61 12.92 o -3 6 2 75.61 72.09 3.56 o -2 6 2 878.15 881.64 11.11 o -1 6 2 8.85 10.16 1.70 o 0 6 2 1077.85 1074.53 13.01 o 1 6 2 194.07 189.63 5.14 o 2 6 2 622.19 625.39 6.94 o 3 6 2 1425.28 1418.42 28.12 o 4 6 2 11.05 10.49 1.09 o 5 6 2 118.38 116.57 1.34 o 6 6 2 13.31 13.79 1.26 o 7 6 2 25.64 26.89 2.89 o 8 6 2 20.71 17.20 2.24 o -7 7 2 50.29 48.96 1.34 o -6 7 2 8.74 10.09 1.21 o -5 7 2 15.08 16.66 1.18 o -4 7 2 23.02 22.91 1.04 o -3 7 2 334.15 332.30 8.53 o -2 7 2 12.12 13.75 2.31 o -1 7 2 587.05 592.81 5.48 o 0 7 2 107.37 111.36 1.77 o 1 7 2 1451.51 1431.31 26.77 o 2 7 2 7.56 10.09 1.16 o 3 7 2 267.12 275.34 5.57 o 4 7 2 8.42 10.58 1.54 o 5 7 2 17.86 18.83 1.51 o 6 7 2 56.61 54.77 2.79 o -3 8 2 39.33 39.45 2.28 o -2 8 2 203.39 210.29 4.52 o -1 8 2 15.22 18.58 1.19 o 0 8 2 303.57 299.55 11.04 o 1 8 2 191.93 200.86 2.73 o 2 8 2 216.60 219.89 2.99 o 3 8 2 283.90 258.29 11.80 o -13 0 3 16.93 14.59 1.75 o -11 0 3 550.89 552.77 10.53 o -9 0 3 2724.56 2791.77 52.39 o -7 0 3 205.21 203.65 13.97 o -5 0 3 2844.79 2940.99 96.51 o -1 0 3 1005.33 914.30 17.46 o 1 0 3 1617.00 1881.17 11.50 o 3 0 3 1286.76 1225.96 13.61 o 5 0 3 2602.56 2684.99 45.50 o 7 0 3 2360.90 2493.14 30.57 o 9 0 3 711.05 727.77 33.02 o 11 0 3 191.12 198.36 2.49 o -13 1 3 7.36 6.42 1.86 o -12 1 3 79.90 83.38 2.35 o -11 1 3 24.34 27.45 1.36 o -10 1 3 1616.65 1644.22 16.54 o -9 1 3 23.30 23.31 1.09 o -8 1 3 1533.10 1504.24 47.38 o -7 1 3 224.87 230.71 2.24 o -6 1 3 327.12 337.53 3.22 o -5 1 3 141.30 149.95 2.95 o -4 1 3 3761.64 3607.39 137.47 o -3 1 3 1467.82 1450.91 39.67 o -2 1 3 17.13 35.74 3.17 o -1 1 3 70.40 66.27 2.58 o 0 1 3 53.08 59.87 1.83 o 1 1 3 9.46 4.94 1.40 o 2 1 3 3423.51 3589.45 31.70 o 3 1 3 4.78 5.17 1.50 o 4 1 3 2141.36 2104.98 29.00 o 5 1 3 1295.39 1359.01 11.02 o 6 1 3 2639.30 2676.64 41.84 o 7 1 3 3.65 2.99 1.20 o 8 1 3 568.67 580.79 16.76 o 9 1 3 496.81 529.51 8.70 o 10 1 3 346.53 336.10 12.54 o 11 1 3 197.94 198.07 8.37 o 12 1 3 39.44 31.14 2.02 o -12 2 3 218.93 217.52 2.87 o -11 2 3 151.59 159.20 2.85 o -10 2 3 385.95 397.20 8.69 o -9 2 3 735.41 776.99 12.49 o -8 2 3 62.57 59.02 1.00 o -7 2 3 389.59 389.83 6.25 o -6 2 3 298.52 301.34 4.63 o -5 2 3 937.59 928.28 11.90 o -4 2 3 1675.14 1724.69 37.61 o -3 2 3 1149.88 978.58 33.33 o -2 2 3 100.53 102.53 2.69 o -1 2 3 670.88 454.35 59.80 o 0 2 3 4023.84 3855.94 69.77 o 1 2 3 3242.75 2949.59 156.37 o 2 2 3 27.79 27.93 1.49 o 3 2 3 1455.16 1464.61 8.35 o 4 2 3 602.71 614.33 4.24 o 5 2 3 1215.77 1168.08 33.52 o 6 2 3 92.26 98.73 1.67 o 7 2 3 215.60 223.63 2.08 o 8 2 3 757.90 735.82 21.89 o 9 2 3 133.12 131.65 5.65 o 10 2 3 264.24 258.57 7.70 o 11 2 3 347.45 321.42 11.42 o 12 2 3 0.60 1.18 1.30 o -12 3 3 132.24 113.98 5.34 o -11 3 3 182.18 181.47 5.29 o -10 3 3 29.65 32.49 0.94 o -9 3 3 60.83 67.80 2.31 o -8 3 3 2.43 6.74 1.08 o -7 3 3 42.51 47.63 1.66 o -6 3 3 260.71 260.57 1.94 o -5 3 3 76.05 76.72 1.46 o -4 3 3 1692.03 1456.31 103.52 o -3 3 3 613.93 605.17 44.54 o -2 3 3 4686.88 4298.48 62.65 o -1 3 3 1043.80 919.33 46.84 o 0 3 3 5645.38 4814.61 122.39 o 1 3 3 289.40 269.73 4.97 o 2 3 3 537.09 509.73 9.35 o 3 3 3 28.49 33.36 1.22 o 4 3 3 14.22 13.07 1.11 o 5 3 3 210.21 200.32 10.20 o 6 3 3 22.57 22.72 1.07 o 7 3 3 188.11 188.40 2.96 o 8 3 3 31.32 30.79 1.02 o 9 3 3 110.58 102.46 1.78 o 10 3 3 496.53 472.52 14.09 o 11 3 3 0.39 1.48 1.06 o -11 4 3 7.61 6.56 1.41 o -10 4 3 29.86 27.94 1.31 o -9 4 3 51.15 53.04 1.84 o -8 4 3 5.45 6.45 1.04 o -7 4 3 171.71 166.36 4.00 o -6 4 3 276.51 283.86 3.73 o -5 4 3 478.75 464.54 8.24 o -4 4 3 118.49 116.78 5.73 o -3 4 3 1674.33 1578.69 37.97 o -2 4 3 10.75 12.91 1.67 o -1 4 3 5090.69 4363.94 200.23 o 0 4 3 84.34 79.06 1.65 o 1 4 3 1712.13 1567.34 27.13 o 2 4 3 1174.33 1127.45 30.10 o 3 4 3 34.53 35.31 3.24 o 4 4 3 0.18 1.15 1.10 o 5 4 3 24.03 24.11 1.59 o 6 4 3 14.16 14.35 1.60 o 7 4 3 11.39 14.15 1.54 o 8 4 3 19.51 21.84 1.21 o 9 4 3 178.53 177.63 2.51 o 10 4 3 66.89 68.20 3.46 o -10 5 3 68.34 67.56 2.15 o -9 5 3 6.83 6.22 1.12 o -8 5 3 368.65 371.67 6.35 o -7 5 3 88.23 90.61 4.55 o -6 5 3 643.56 655.22 19.45 o -5 5 3 705.03 698.90 10.69 o -4 5 3 22.54 23.49 1.15 o -3 5 3 190.16 191.81 3.91 o -2 5 3 333.14 333.65 5.21 o -1 5 3 3.33 5.63 1.36 o 0 5 3 801.10 783.84 10.25 o 1 5 3 665.52 643.01 4.14 o 2 5 3 467.70 451.44 4.78 o 3 5 3 313.58 332.24 6.50 o 4 5 3 586.43 561.56 45.23 o 5 5 3 11.44 17.87 1.63 o 6 5 3 282.99 303.17 3.47 o 7 5 3 2.05 6.45 1.01 o 8 5 3 134.45 132.68 4.79 o 9 5 3 414.51 388.03 23.21 o -9 6 3 294.21 297.69 6.09 o -8 6 3 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