Received 6 November 2013
aSchool of Chemistry and Chemical Engineering, Shandong University, Jinan 250100, People's Republic of China,bSchool of Chemistry and Chemical Engineering, Taian University, Taian 271021, People's Republic of China, and cSchool of Chemistry and Chemical Engineering, Liaocheng University, Liaocheng 252000, People's Republic of China
Correspondence e-mail: firstname.lastname@example.org
The title compound, C17H19NO3S, was synthesized from 4-benzhydrylideneamino-12-hydroxy-[2.2]paracyclophane and methanesulfonyl chloride. In the molecule, the distance between the centroids of two aromatic rings is 2.960 (5) Å. In the crystal, weak N-HO and C-HO hydrogen bonds link the molecules into layers parallel to the ac plane.
For background to [2.2]paracyclophane, see: Cram et al. (1959); Liebman & Greenberg (1976); Dyson et al. (1998). For its synthesis and applications in catalysis, see: Hou et al. (2000); Duan et al. (2008, 2012). For a related structure, see: Ma et al. (2012).
Data collection: SMART (Bruker, 2007); cell refinement: SAINT (Bruker, 2007); data reduction: SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: SHELXTL (Sheldrick, 2008); software used to prepare material for publication: SHELXTL.
Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: CV5436 ).
Financial support from Shandong Province Natural Science Foundation (ZR2012BL08) is gratefully acknowledged.
Bruker (2007). SMART, SAINT and SADABS. Bruker AXS Inc., Madison, Wisconsin, USA.
Cram, D. J. (1959). Rec. Chem. Prog. 20, 71-93.
Duan, W. Z., Ma, Y. D., Qu, B., Zhao, L., Chen, J. Q. & Song, C. (2012). Tetrahedron Asymmetry, 23, 1369-1375.
Duan, W. Z., Ma, Y. D., Xia, H. Q., Liu, X. Y., Ma, Q. S. & Sun, J. S. (2008). J. Org. Chem. 73, 4330-4333.
Dyson, P. J., Johnson, B. F. G. & Martin, C. M. (1998). Coord. Chem. Rev. 175, 59-89.
Flack, H. D. (1983). Acta Cryst. A39, 876-881.
Hou, X. L., Wu, X. W., Dai, L. X., Cao, B. X. & Sun, J. (2000). Chem. Commun. pp. 1195-1196.
Liebman, J. F. & Greenberg, A. (1976). Chem. Rev. 76, 311-365.
Ma, K., Duan, W., He, F. & Ma, Y. (2012). Acta Cryst. E68, o1380.
Sheldrick, G. M. (2008). Acta Cryst. A64, 112-122.