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Acta Cryst. (2014). E70, m9-m10  [ doi:10.1107/S1600536813032510 ]

(1,4,7,10,13,16-Hexaoxa­cyclo­octa­decane-[kappa]6O)bis­(tetra­hydro­furan-[kappa]O)potassium bis­[(1,2,3,4-[eta])-anthracene]cobalt(-I) tetra­hydro­furan monosolvate

H. He, W. Klein and T. F. Fässler


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Alert level B PLAT360_ALERT_2_B Short C(sp3)-C(sp3) Bond C45 - C46 ... 1.33 Ang.
Alert level C GOODF01_ALERT_2_C The least squares goodness of fit parameter lies outside the range 0.80 <> 2.00 Goodness of fit given = 0.765 PLAT090_ALERT_3_C Poor Data / Parameter Ratio (Zmax > 18) ........ 8.61 PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density .... 2.57 PLAT230_ALERT_2_C Hirshfeld Test Diff for C10 -- C11 .. 5.2 su PLAT230_ALERT_2_C Hirshfeld Test Diff for C13 -- C14 .. 5.2 su PLAT243_ALERT_4_C High 'Solvent' Ueq as Compared to Neighbors of C43 Check PLAT243_ALERT_4_C High 'Solvent' Ueq as Compared to Neighbors of C45 Check PLAT243_ALERT_4_C High 'Solvent' Ueq as Compared to Neighbors of C48 Check PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of O8 Check PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C46 Check PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C47 Check PLAT341_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0062 Ang. PLAT411_ALERT_2_C Short Inter H...H Contact H7A .. H17A .. 2.14 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 9.857 Check PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.905 Check PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 10 Why ? PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 3
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ Please Check PLAT302_ALERT_4_G Anion/Solvent Disorder ............ Percentage = 31 Note PLAT764_ALERT_4_G Overcomplete CIF Bond List Detected (Rep/Expd) . 1.10 Ratio PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 4 C4 H8 O PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... Please Check
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 17 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 9 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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