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Acta Cryst. (2014). E70, o72  [ doi:10.1107/S1600536813033734 ]

N,N,2,4,6-Penta­methyl­anilinium hexa­fluoro­phosphate-1,4,7,10,13,16-hexa­oxa­cyclo­octa­decane (2/1)

Y. Q. Chang, Y. Zhang and H. L. Lian


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Alert level C PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0063 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 17.930 Check PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 3.228 Check PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 7 Why ? PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 2
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT007_ALERT_5_G Number of Unrefined Donor-H Atoms .............. 1 Why ? PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ Please Check PLAT199_ALERT_1_G Reported _cell_measurement_temperature ..... (K) 293 Check PLAT200_ALERT_1_G Reported _diffrn_ambient_temperature ..... (K) 293 Check PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of P1 Check PLAT380_ALERT_4_G Incorrectly? Oriented X(sp2)-Methyl Moiety ..... C13 Check PLAT380_ALERT_4_G Incorrectly? Oriented X(sp2)-Methyl Moiety ..... C14 Check PLAT380_ALERT_4_G Incorrectly? Oriented X(sp2)-Methyl Moiety ..... C15 Check
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 9 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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