Acta Crystallographica Section E

Structure Reports Online

Volume 70, Part 1 (January 2014)

organic compounds

sj5364 scheme

Acta Cryst. (2014). E70, o13    [ doi:10.1107/S160053681303242X ]

Dimethyl 2-[2-(2,4,6-tri­chloro­phen­yl)hydrazin-1-yl­idene]butane­dioate

M. K. Usha, S. Shetty, B. Kalluraya, R. Kant, V. K. Gupta and D. Revannasiddaiah

Abstract: In the title compound, C12H11Cl3N2O4, the dihedral angle between the aromatic ring and the hydrazine (NH-N=C) grouping is 52.2 (3)°. The butanedioate groups exhibit planar conformations. An intra­molecular N-H...O hydrogen bond links the N-H group of the hydrazine to one of the meth­oxy groups of the butane­dioate moiety. In the crystal, mol­ecules are linked by C-H...O hydrogen bonds and [pi]-[pi] inter­actions are also observed [centroid-centroid separation = 3.535 (1) Å].

CCDC reference: 967565

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