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Acta Cryst. (2014). E70, m20  [ doi:10.1107/S1600536813033515 ]

Iodido­bis­(morpholine-4-carbodi­thio­ato-[kappa]2S,S')(1,10-phenanthroline-[kappa]2N,N')bis­muth(III)

F. Li, H. Yin and G. Wu


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Alert level C PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Bi1 -- S2 .. 6.1 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Bi1 -- S4 .. 5.1 su PLAT241_ALERT_2_C High Ueq as Compared to Neighbors for ..... S2 Check PLAT241_ALERT_2_C High Ueq as Compared to Neighbors for ..... S4 Check PLAT242_ALERT_2_C Low Ueq as Compared to Neighbors for ..... Bi1 Check PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0127 Ang. PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -0.703 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 17 PLAT973_ALERT_2_C Large Calcd. Positive Residual Density on Bi1 1.13 eA-3
Alert level G PLAT003_ALERT_2_G Number of Uiso or Uij Restrained non-H Atoms ... 9 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Bi1 -- I1 .. 20.3 su PLAT860_ALERT_3_G Number of Least-Squares Restraints ............. 162 Note PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 53 % PLAT910_ALERT_3_G Missing # of FCF Reflections Below Th(Min) ..... 1 Why ?
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 9 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 8 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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