Acta Crystallographica Section E

Structure Reports Online

Volume 70, Part 1 (January 2014)

organic compounds

sj5378 scheme

Acta Cryst. (2014). E70, o59-o60    [ doi:10.1107/S1600536813033424 ]


Z.-Y. Li, P. Wang and X. Chen

Abstract: The title mol­ecule, C24H25NOSi, is a hydrolysis product of the reaction between 9-tri­methyl­silyfluorenyl lithium and 2-meth­oxy­benzo­nitrile. The fluorene ring system is substanti­ally planar, with an r.m.s. deviation of 0.0288 Å from the best-fit plane through its 13 C atoms. This plane forms a dihedral angle of 58.07 (7)° with the 2-meth­oxy­benzyl­amine ring plane. In the crystal, mol­ecules are linked by N-H...[pi] and C-H...[pi] inter­actions, which leads to the formation of two-dimensional network lying parallel to the bc plane.

CCDC reference: 976209

htmldisplay filedownload file

Hyper-Text Markup Language (HTML) file (82.7 kbytes)
[ doi:10.1107/S1600536813033424/sj5378sup0.html ]
Supplementary materials

cmldisplay filedownload file

Chemical Markup Language (CML) file (7.8 kbytes)
[ doi:10.1107/S1600536813033424/sj5378Isup3.cml ]
Supplementary material


To open or display or play some files, you may need to set your browser up to use the appropriate software. See the full list of file types for an explanation of the different file types and their related mime types and, where available links to sites from where the appropriate software may be obtained.

The download button will force most browsers to prompt for a file name to store the data on your hard disk.

Where possible, images are represented by thumbnails.

 bibliographic record in  format

  Find reference:   Volume   Page   
  Search:     From   to      Advanced search

Copyright © International Union of Crystallography
IUCr Webmaster