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Acta Cryst. (2014). E70, m14-m15  [ doi:10.1107/S1600536813032480 ]

Tri-[mu]-chlorido-bis­[([eta]5-penta­methyl­cyclo­penta­dien­yl)rhodium(III)] hexa­fluorido­phosphate from synchrotron radiation

L. Ezzedinloo, S. Shrestha, M. Bhadbhade and S. Colbran

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checkCIF/PLATON results

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Alert level B Crystal system given = triclinic PLAT019_ALERT_1_B Check _diffrn_measured_fraction_theta_full/_max 0.972 PLAT028_ALERT_3_B _diffrn_measured_fraction_theta_max Low ....... 0.896 PLAT911_ALERT_3_B Missing # FCF Refl Between THmin & STh/L= 0.595 480
Alert level C PLAT241_ALERT_2_C High Ueq as Compared to Neighbors for ..... Cl2 Check PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of P1 Check PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 3.2 Note PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 42
Alert level G ABSMU01_ALERT_1_G Calculation of _exptl_absorpt_correction_mu not performed for this radiation type. PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.03000 Deg. PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Rh1A -- Cl2 .. 5.6 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Rh1A -- Cl3 .. 5.8 su PLAT380_ALERT_4_G Incorrectly? Oriented X(sp2)-Methyl Moiety ..... C6A Check PLAT380_ALERT_4_G Incorrectly? Oriented X(sp2)-Methyl Moiety ..... C10A Check PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 24 PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 94 % PLAT910_ALERT_3_G Missing # of FCF Reflections Below Th(Min) ..... 2 Why ? PLAT984_ALERT_1_G The Rh-f'= -1.118 Deviates from the B&C-Value -1.096
0 ALERT level A = Most likely a serious problem - resolve or explain 3 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 11 ALERT level G = General information/check it is not something unexpected 4 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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