Acta Crystallographica Section E

Structure Reports Online

Volume 70, Part 5 (May 2014)

organic compounds

bt6973 scheme

Acta Cryst. (2014). E70, o539    [ doi:10.1107/S1600536814007594 ]


Z. Moussa, H. T. Al-Masri, A. Shraim and M. Fettouhi

Abstract: The title compound, C23H24O3, was obtained in a one-step (60% yield) synthesis from 1,1,1-tris(hydroxymethyl)ethane. It features a tripodal ligand capable of complexing metal centres. One of the three conformations involving the methyl group, the central C-C bond and the phenoxy substituents is antiperiplanar while the two others are synclinal [the corresponding C-C-C-O torsion angles are -174.6 (1), -53.2 (2) and -47.3 (2)°]. In the crystal, C-H...O inter­actions link the molecules into [010] chains.

CCDC reference: 942596

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