[Open access]

[Contents scheme]

Acta Cryst. (2014). E70, m190-m191
[ doi:10.1107/S1600536814009064 ]

Bis(2,2'-bipyridyl-[kappa]2N,N')chloridonickel(II) nitrate trihydrate

M. Boutebdja, A. Beghidja, C. Beghidja, Z. Setifi and H. Merazig


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of N5 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 13 Why ? PLAT976_ALERT_2_C Check Calcd Residual Density 0.67A From O2W -0.42 eA-3
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 9 Note PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT007_ALERT_5_G Number of Unrefined Donor-H Atoms .............. 6 Why ? PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ni1 -- N1 .. 6.1 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ni1 -- N4 .. 6.2 su PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 3 Note H2 O PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 4 Note H2 O PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 5 Note H2 O PLAT860_ALERT_3_G Number of Least-Squares Restraints ............. 9 Note PLAT910_ALERT_3_G Missing # of FCF Reflections Below Th(Min) ..... 3 Why ? PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 7 Note
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 11 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 5 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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