[Open access]

[Contents scheme]

Acta Cryst. (2014). E70, o563-o564
[ doi:10.1107/S1600536814007934 ]

1-(2,3,4,5,6-Penta­methyl­benz­yl)-2-(pyridin-2-yl)-1H-benzimidazole

F. Angay, Ö. Çelik, O. Barlik and M. Ulusoy


Key indicators

checkCIF/PLATON results

No syntax errors found



Alert level A PLAT015_ALERT_5_A No _shelx_hkl_file record in SHELXL20xy CIF ... Please Do !
Alert level C PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H20A PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H20B PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H20C PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H21A PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H21B PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H21C PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H22A PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H22B PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H22C PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H23A PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H23B PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H23C PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H24A PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H24B PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H24C PLAT412_ALERT_2_C Short Intra XH3 .. XHn H23B .. H24B .. 1.80 Ang. PLAT742_ALERT_1_C Angle Calc 109.5(4), Rep 109.50 ...... Missing su C15 -C20 -H20A 1.555 1.555 1.555 # 61 PLAT742_ALERT_1_C Angle Calc 109.4(6), Rep 109.50 ...... Missing su C15 -C20 -H20B 1.555 1.555 1.555 # 62 PLAT742_ALERT_1_C Angle Calc 109.5(10), Rep 109.50 ...... Missing su H20A -C20 -H20B 1.555 1.555 1.555 # 63 PLAT742_ALERT_1_C Angle Calc 109.5(6), Rep 109.50 ...... Missing su C15 -C20 -H20C 1.555 1.555 1.555 # 64 PLAT742_ALERT_1_C Angle Calc 109.4(10), Rep 109.50 ...... Missing su H20A -C20 -H20C 1.555 1.555 1.555 # 65 PLAT742_ALERT_1_C Angle Calc 109.6(9), Rep 109.50 ...... Missing su H20B -C20 -H20C 1.555 1.555 1.555 # 66 PLAT742_ALERT_1_C Angle Calc 109.5(5), Rep 109.50 ...... Missing su C16 -C21 -H21A 1.555 1.555 1.555 # 67 PLAT742_ALERT_1_C Angle Calc 109.4(8), Rep 109.50 ...... Missing su C16 -C21 -H21B 1.555 1.555 1.555 # 68 PLAT742_ALERT_1_C Angle Calc 109.4(13), Rep 109.50 ...... Missing su H21A -C21 -H21B 1.555 1.555 1.555 # 69 PLAT742_ALERT_1_C Angle Calc 109.5(6), Rep 109.50 ...... Missing su C16 -C21 -H21C 1.555 1.555 1.555 # 70 PLAT742_ALERT_1_C Angle Calc 109.5(12), Rep 109.50 ...... Missing su H21A -C21 -H21C 1.555 1.555 1.555 # 71 PLAT742_ALERT_1_C Angle Calc 109.5(12), Rep 109.50 ...... Missing su H21B -C21 -H21C 1.555 1.555 1.555 # 72 PLAT742_ALERT_1_C Angle Calc 109.5(8), Rep 109.50 ...... Missing su C17 -C22 -H22A 1.555 1.555 1.555 # 73 PLAT742_ALERT_1_C Angle Calc 109.5(4), Rep 109.50 ...... Missing su C17 -C22 -H22B 1.555 1.555 1.555 # 74 PLAT742_ALERT_1_C Angle Calc 109.4(14), Rep 109.50 ...... Missing su H22A -C22 -H22B 1.555 1.555 1.555 # 75 PLAT742_ALERT_1_C Angle Calc 109.5(7), Rep 109.50 ...... Missing su C17 -C22 -H22C 1.555 1.555 1.555 # 76 PLAT742_ALERT_1_C Angle Calc 109.5(11), Rep 109.50 ...... Missing su H22A -C22 -H22C 1.555 1.555 1.555 # 77 PLAT742_ALERT_1_C Angle Calc 109.5(11), Rep 109.50 ...... Missing su H22B -C22 -H22C 1.555 1.555 1.555 # 78 PLAT742_ALERT_1_C Angle Calc 109.5(7), Rep 109.50 ...... Missing su C18 -C23 -H23A 1.555 1.555 1.555 # 79 PLAT742_ALERT_1_C Angle Calc 109.5(5), Rep 109.50 ...... Missing su C18 -C23 -H23B 1.555 1.555 1.555 # 80 PLAT742_ALERT_1_C Angle Calc 109.5(12), Rep 109.50 ...... Missing su H23A -C23 -H23B 1.555 1.555 1.555 # 81 PLAT742_ALERT_1_C Angle Calc 109.5(6), Rep 109.50 ...... Missing su C18 -C23 -H23C 1.555 1.555 1.555 # 82 PLAT742_ALERT_1_C Angle Calc 109.3(11), Rep 109.50 ...... Missing su H23A -C23 -H23C 1.555 1.555 1.555 # 83 PLAT742_ALERT_1_C Angle Calc 109.7(11), Rep 109.50 ...... Missing su H23B -C23 -H23C 1.555 1.555 1.555 # 84 PLAT742_ALERT_1_C Angle Calc 109.5(5), Rep 109.50 ...... Missing su C19 -C24 -H24A 1.555 1.555 1.555 # 85 PLAT742_ALERT_1_C Angle Calc 109.6(7), Rep 109.50 ...... Missing su C19 -C24 -H24B 1.555 1.555 1.555 # 86 PLAT742_ALERT_1_C Angle Calc 109.3(11), Rep 109.50 ...... Missing su H24A -C24 -H24B 1.555 1.555 1.555 # 87 PLAT742_ALERT_1_C Angle Calc 109.5(5), Rep 109.50 ...... Missing su C19 -C24 -H24C 1.555 1.555 1.555 # 88 PLAT742_ALERT_1_C Angle Calc 109.6(10), Rep 109.50 ...... Missing su H24A -C24 -H24C 1.555 1.555 1.555 # 89 PLAT742_ALERT_1_C Angle Calc 109.5(11), Rep 109.50 ...... Missing su H24B -C24 -H24C 1.555 1.555 1.555 # 90 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 7.506 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 6 Why ?
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT066_ALERT_1_G Predicted and Reported Tmin&Tmax Range Identical ? Check PLAT910_ALERT_3_G Missing # of FCF Reflections Below Th(Min) ..... 2 Why ? PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... Please Check
1 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 48 ALERT level C = Check. Ensure it is not caused by an omission or oversight 4 ALERT level G = General information/check it is not something unexpected 31 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 15 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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