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[Contents scheme]

Acta Cryst. (2014). E70, m176-m177
[ doi:10.1107/S1600536814007818 ]

Bis{[mu]-cis-1,3-bis­[(di-tert-butyl­phosphan­yl)­oxy]cyclo­hexane-[kappa]2P:P'}bis­[carbonylnickel(0)] including an unknown solvent molecule

K. J. Jonasson and O. F. Wendt


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checkCIF/PLATON results

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Alert level C PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 11.329 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 3 Why ?
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ni1 -- C7 .. 6.9 su PLAT605_ALERT_4_G Structure Contains Solvent Accessible VOIDS of . 170 A   3 PLAT793_ALERT_4_G The Model has Chirality at C2 ............. R Verify PLAT793_ALERT_4_G The Model has Chirality at C6 ............. S Verify PLAT869_ALERT_4_G ALERTS Related to the use of SQUEEZE Suppressed ! Info PLAT910_ALERT_3_G Missing # of FCF Reflections Below Th(Min) ..... 4 Why ? PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 734 Note PLAT952_ALERT_5_G Reported and Calculated Lmax Values Differ by .. 3 Check PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... Please Check
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 2 ALERT level C = Check. Ensure it is not caused by an omission or oversight 10 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 5 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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