[Open access]

[Contents scheme]

Acta Cryst. (2014). E70, m160-m161
[ doi:10.1107/S160053681400631X ]

Bis[bis­(2,2'-bi­pyridine-[kappa]2N,N')(carbon­ato-[kappa]2O,O')cobalt(III)] 2-{4-[(carboxyl­atometh­yl)carbamo­yl]benz­amido}­acetate hexa­hydrate

N.-P. Pook, M. Gjikaj and A. Adam


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT068_ALERT_1_C Reported F000 Differs from Calcd (or Missing)... Please Check PLAT352_ALERT_3_C Short N-H (X0.87,N1.01A) N5 - H5A ... 0.74 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H3 .. O4 .. 2.64 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.335 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 57 Why ? PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1 Note
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ Please Check PLAT045_ALERT_1_G Calculated and Reported Z Differ by ............ 2.00 Ratio PLAT164_ALERT_4_G Nr. of Refined C-H H-Atoms in Heavy-Atom Struct. 20 Note PLAT764_ALERT_4_G Overcomplete CIF Bond List Detected (Rep/Expd) . 1.11 Ratio PLAT910_ALERT_3_G Missing # of FCF Reflections Below Th(Min) ..... 3 Why ? PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 19 Note
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 7 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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